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MassMS-KW-0093 4-amino-3-nitrophenol C6H6N2O3 (Mass of molecular ion: 154)
Source Temperature: 130 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 2.8 27.0 1.7 28.0 3.5 39.0 2.7 40.0 1.0 41.0 1.2 50.0 1.1 51.0 3.0 52.0 10.0 53.0 10.3 53.5 1.4 54.0 3.0 55.0 1.4 63.0 2.5 65.0 1.0 67.0 1.4 68.0 17.1 77.0 1.7 78.0 1.2 79.0 2.3 80.0 5.8 81.0 11.2 90.0 1.3 91.0 1.2 96.0 2.2 107.0 3.4 108.0 40.1 109.0 3.1 124.0 1.8 137.0 1.1 154.0 100.0 155.0 7.8
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C6 H6 N2 O3 0.035 g : 0.5 ml DMSO-d6 4-amino-3-nitrophenol 
Assign. Shift(ppm)
A 9.31 B 7.330 C 7.08 D 7.047 E 6.954
Hz ppm Int.3720.25 9.309 1000 2931.21 7.335 408 2928.31 7.328 412 2829.59 7.081 404 2823.03 7.064 237 2820.28 7.057 203 2814.03 7.042 306 2811.13 7.034 291 2782.44 6.963 478 2773.44 6.940 309
in CDCl3
KBr disk
Nujol
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