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6090-09-1

4-acetyl-1-methyl-1-cyclohexene

Product Name 4-acetyl-1-methyl-1-cyclohexene

CAS6090-09-1

MFC9H14O

MW138.21

More

  • 6090-09-1_ms_1
    Mass

    MS-IW-1774          
    4-acetyl-1-methylcyclohexene
    C9H14O              (Mass of molecular ion:    138)
    

       Source Temperature: 240 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          15.0       2.5
          27.0       9.6
          28.0       1.0
          29.0       4.9
          38.0       1.1
          39.0      15.2
          40.0       3.0
          41.0      17.2
          42.0       1.7
          43.0      79.3
          44.0       2.1
          45.0       5.4
          50.0       1.7
          51.0       5.2
          52.0       2.3
          53.0      12.9
          54.0       1.9
          55.0      25.8
          56.0       1.2
          63.0       1.7
          65.0       5.7
          66.0       1.7
          67.0      44.6
          68.0      12.0
          69.0       2.4
          71.0       3.2
          77.0      15.1
          78.0       3.1
          79.0      25.2
          80.0      14.4
          81.0      11.6
          82.0       2.1
          83.0       1.7
          91.0      10.2
          92.0       3.0
          93.0      21.1
          94.0      15.4
          95.0     100.0
          96.0       9.2
          97.0       1.5
         105.0      13.4
         106.0       1.3
         107.0       1.1
         109.0       7.1
         110.0       1.7
         120.0       2.4
         121.0       1.5
         123.0      42.8
         124.0       4.0
         137.0       1.6
         138.0      70.6
         139.0       7.2
    

400 MHz in CDCl3

  • 6090-09-1_1hnmr_0

    1H NMR 399.65 MHz
    C9 H14 O 0.05 ml : 0.5 ml CDCl3
    4-acetyl-1-methylcyclohexene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 5.388 B 2.532 C 2.174 D 2.15 E 2.12 F 1.95 G 1.649 J 1.60

         Hz     ppm     Int.
    

       2156.74   5.397     68
       2155.40   5.394     80
       2153.93   5.390     83
       2152.34   5.386     76
       2150.88   5.382     62
       1015.26   2.541     41
       1009.28   2.526     44
        869.14   2.175   1000
        865.72   2.167     88
        863.28   2.161     95
        862.30   2.158    119
        860.23   2.153    119
        858.15   2.148    101
        853.76   2.137     63
        851.44   2.131     61
        848.51   2.124     47
        797.85   1.997    110
        797.12   1.995    108
        795.90   1.992    116
        794.56   1.989    105
        793.21   1.985     92
        791.87   1.982     77
        782.96   1.960     65
        781.98   1.957     69
        780.15   1.953     54
        778.93   1.950     50
        777.22   1.945     51
        776.00   1.942     47
        659.67   1.651    352
        658.94   1.649    343
        653.20   1.635     48
        648.32   1.623     58
        642.70   1.609     52
        641.48   1.606     49
        637.94   1.597     47
        636.96   1.594     48
        631.96   1.582     50
        626.59   1.568     46
    

in CDCl3

  • 6090-09-1_13cnmr_0

liquid film

  • 6090-09-1_ir1_0