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2-Chlorobenzamide

Product Name 2-Chlorobenzamide

CAS609-66-5

MFC7H6ClNO

MW155.58

¹³CNMR

Mass

MS-NW-1879          
o-chlorobenzamide
C7H6ClNO            (Mass of molecular ion:    155)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       2.0
      27.0       1.1
      28.0       1.5
      37.0       2.7
      37.5       1.0
      38.0       3.9
      39.0       2.4
      44.0      10.7
      45.5       1.3
      49.0       1.8
      50.0      15.6
      51.0       9.4
      52.0       1.3
      61.0       1.3
      63.0       1.6
      63.5       1.8
      65.0       1.8
      73.0       2.2
      74.0       7.9
      75.0      26.0
      76.0       7.9
      77.0       8.7
      84.0       1.4
      85.0       3.1
      87.0       1.0
      90.0       1.0
     102.0       1.4
     110.0       1.1
     111.0      37.7
     112.0       5.7
     113.0      12.3
     114.0       1.6
     137.0       1.1
     139.0     100.0
     140.0       7.6
     141.0      31.5
     142.0       2.6
     155.0      57.7
     156.0       4.6
     157.0      18.6
     158.0       1.5

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₆ Cl N O	saturated in CDCl₃
o-chlorobenzamide

    Assign.     Shift(ppm)

      A             7.773
      B             7.42
      C             7.40
      D             7.35
      E     *1      6.56
      F     *1      6.42
     
     J(A,C)=1.4HZ. J(A,D)=7.6HZ.

     Hz     ppm     Int.

   3118.16   7.803     44
   3116.70   7.799     59
   3110.84   7.784    517
   3109.62   7.781    519
   3109.25   7.780    518
   3103.39   7.766    585
   3101.93   7.762    563
   3095.21   7.745     42
   2984.25   7.468     41
   2983.76   7.466     42
   2983.15   7.465     45
   2982.18   7.462     48
   2981.69   7.461     46
   2981.32   7.460     49
   2980.71   7.459     54
   2980.35   7.458     52
   2979.86   7.457     59
   2979.13   7.455     67
   2978.03   7.452     82
   2973.27   7.440    288
   2972.05   7.437    358
   2969.85   7.432    182
   2965.33   7.420    872
   2964.11   7.417   1000
   2961.43   7.411    523
   2961.06   7.410    528
   2955.69   7.396    657
   2953.98   7.392    631
   2948.00   7.377    348
   2946.17   7.372    358
   2943.12   7.365    495
   2941.41   7.360    445
   2935.79   7.346    544
   2934.20   7.342    517
   2928.59   7.328    238
   2927.12   7.325    212
   2923.83   7.316     65
   2923.34   7.315     62
   2922.97   7.314     56
   2921.02   7.309     45
   2919.92   7.307     45
   2622.56   6.563    136
   2564.21   6.417    132

¹H NMR	89.56 MHz
C₇ H₆ Cl N O	0.038 g : 0.5 ml CDCl₃
o-chlorobenzamide

    Assign.     Shift(ppm)

      A             7.75
      B          7.60 to 7.12
      C             6.5

     Hz     ppm     Int.

    699.31   7.809    146
    698.75   7.803    157
    698.06   7.795    155
    697.31   7.786    140
    696.50   7.777    126
    694.56   7.756    217
    692.44   7.732    163
    691.38   7.720    190
    690.88   7.715    189
    690.56   7.711    186
    670.38   7.486     63
    669.94   7.481     74
    661.75   7.389   1000
    655.88   7.324    241
    655.56   7.320    242
    653.06   7.292    140
    652.56   7.287    146
    650.94   7.269    183
    583.94   6.521     86

in CDCl3

KBr disc

nujol mull

4880 A,200 M,powder

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