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MassMS-NW-0840 2,3-dichloroaniline C6H5Cl2N (Mass of molecular ion: 161)
Source Temperature: 280 °C Sample Temperature: 150 °C Reservoir, 75 eV
28.0 4.7 36.0 1.0 37.0 3.6 38.0 3.7 39.0 3.9 41.0 2.7 42.0 1.2 43.0 1.0 44.5 5.0 45.0 1.1 45.5 1.5 49.0 1.2 50.0 1.5 51.0 1.1 52.0 3.8 57.0 1.1 61.0 3.4 62.0 6.1 62.5 6.3 63.0 14.0 63.5 2.1 64.0 4.1 65.0 3.5 72.0 2.0 73.0 4.6 74.0 1.8 75.0 1.9 80.5 6.0 81.5 3.7 86.0 1.5 88.0 1.2 89.0 3.4 90.0 26.1 91.0 5.0 97.0 2.0 98.0 2.8 99.0 12.5 100.0 2.1 101.0 4.2 124.0 1.4 125.0 7.4 126.0 11.5 127.0 3.4 128.0 3.7 133.0 3.9 134.0 2.9 135.0 2.9 136.0 1.9 160.0 1.0 161.0 100.0 162.0 7.8 163.0 63.9 164.0 4.5 165.0 10.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H5 Cl2 N 0.04 ml : 0.5 ml CDCl3 2,3-dichloroaniline 
Assign. Shift(ppm)
A 6.936 B 6.827 C 6.626 D 4.1
Hz ppm Int.631.63 7.053 219 624.19 6.970 364 623.69 6.964 599 616.31 6.882 1000 614.44 6.861 609 612.25 6.837 914 606.50 6.772 321 604.31 6.748 147 597.13 6.668 684 594.94 6.643 485 589.75 6.585 399 587.56 6.561 355 369.06 4.121 83
in CDCl3
liquid film
OXIDATION WITH PERBENZOIC ACID
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