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MS-KW-0165 3-chloro-o-xylene C8H9Cl (Mass of molecular ion: 140)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 2.5 38.0 1.3 39.0 4.4 50.0 3.6 51.0 14.3 51.5 1.1 52.0 2.5 53.0 1.5 62.0 1.8 63.0 4.3 65.0 1.5 69.0 1.9 70.0 1.0 73.0 1.4 74.0 1.5 75.0 2.4 76.0 1.2 77.0 14.2 78.0 5.2 79.0 8.0 89.0 2.7 91.0 1.4 99.0 1.2 101.0 1.3 102.0 2.3 103.0 12.9 104.0 4.4 105.0 100.0 106.0 9.4 125.0 15.0 126.0 1.1 127.0 4.8 139.0 6.0 140.0 36.9 141.0 5.2 142.0 11.8 143.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H9 Cl 0.05 ml : 0.5 ml CDCl3 3-chloro-o-xylene Assign. Shift(ppm)
A 7.173 B 6.99 C 6.96 D *1 2.284 E *1 2.264
Hz ppm Int.
2871.22 7.185 112 2869.75 7.181 100 2869.14 7.180 103 2863.89 7.166 140 2861.94 7.162 130 2801.39 7.010 44 2799.44 7.005 68 2799.07 7.004 68 2793.70 6.991 233 2791.26 6.985 348 2783.57 6.966 191 2776.12 6.947 58 921.14 2.305 42 920.65 2.304 45 912.96 2.285 1000 904.91 2.265 901 904.54 2.264 901
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