5-Nitroisoquinoline

Mass

MS-NW-6732          
5-nitroisoquinoline
C9H6N2O2            (Mass of molecular ion:    174)

   Source Temperature: 160 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      16.0       1.4
      17.0       1.4
      18.0       2.3
      26.0       5.4
      27.0       4.3
      28.0       6.4
      29.0       1.2
      30.0      28.6
      36.0       1.5
      37.0      12.6
      38.0      15.6
      39.0      16.3
      40.0       2.6
      41.0       1.2
      46.0       6.1
      48.0       1.2
      49.0       8.4
      49.5       1.1
      50.0      40.0
      51.0      55.0
      52.0       8.1
      53.0       1.5
      60.0       2.5
      61.0      16.1
      62.0      29.0
      63.0      40.8
      64.0       7.2
      65.0       3.1
      72.0       1.0
      73.0       8.2
      74.0      66.0
      75.0      99.0
      76.0      19.2
      77.0      26.4
      78.0       4.5
      81.0       5.7
      84.0       1.0
      85.0       3.3
      86.0       6.2
      87.0       7.6
      88.0       7.9
      89.0      61.2
      90.0      10.3
      91.0      36.1
      92.0       4.5
      97.0       2.9
      98.0      14.6
      99.0      10.1
     100.0      14.2
     101.0      69.7
     102.0      14.3
     103.0      11.8
     104.0       2.2
     114.0       2.4
     115.0       3.3
     116.0     100.0
     117.0      14.6
     118.0       6.9
     119.0       7.6
     126.0       1.1
     127.0       7.7
     128.0      38.5
     129.0       6.6
     130.0       2.8
     144.0       8.5
     145.0       2.9
     146.0       1.5
     147.0       7.7
     158.0       1.2
     173.0       1.5
     174.0      36.6
     175.0       4.4

Parameter ppm Hz D(A) 9.39 D(B) 8.75 D(C) 8.46 D(D) 8.59 D(E) 7.72 D(F) 8.36 J(B,C) 5.8 J(B,D) 0.0 J(B,E) 0.0 J(B,F) 0.0 J(C,D) 0.0 J(C,E) 0.0 J(C,F) 0.8 J(D,E) 8.5 J(D,F) 1.8 J(E,F) 8.5 ARMAREGO,W.L.F. & BATTERHAM,T.J. J.CHEM.SOC. B 1966 750

     Hz     ppm     Int.

   2817.01   9.390   1000
   2627.99   8.760    469
   2622.21   8.741    535
   2582.23   8.607    247
   2580.44   8.601    259
   2573.74   8.579    263
   2571.95   8.573    277
   2541.18   8.471    313
   2540.44   8.468    324
   2535.39   8.451    274
   2534.64   8.449    285
   2513.62   8.379    157
   2512.85   8.376    161
   2511.83   8.373    162
   2511.07   8.370    145
   2505.11   8.350    172
   2504.35   8.348    179
   2503.32   8.344    175
   2502.58   8.342    157
   2324.33   7.748    271
   2315.85   7.719    500
   2307.36   7.691    232