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MassMS-IW-9682 6-hydroxy-L-norleucine C6H13NO3 (Mass of molecular ion: 147)
Source Temperature: 190 °C Sample Temperature: 200 °C Direct, 75 eV
15.0 3.8 16.0 1.3 17.0 11.0 18.0 53.1 19.0 1.0 25.0 1.4 26.0 11.4 27.0 27.7 28.0 87.3 29.0 21.5 30.0 26.9 31.0 10.0 37.0 1.7 38.0 3.5 39.0 18.6 40.0 6.4 41.0 37.1 42.0 24.2 43.0 68.5 44.0 11.2 45.0 2.4 46.0 6.7 50.0 3.6 51.0 5.4 52.0 8.5 53.0 8.0 54.0 15.4 55.0 29.8 56.0 100.0 57.0 24.6 58.0 1.5 63.0 1.1 64.0 1.3 65.0 3.7 66.0 6.7 67.0 16.9 68.0 4.6 69.0 3.8 70.0 2.9 71.0 4.3 72.0 2.9 73.0 1.7 74.0 21.7 75.0 3.9 78.0 2.3 79.0 5.3 80.0 3.8 81.0 2.9 82.0 11.1 83.0 10.8 84.0 30.0 85.0 39.1 86.0 2.6 87.0 1.5 91.0 1.5 92.0 1.6 93.0 7.4 94.0 1.9 100.0 1.5 101.0 1.8 102.0 27.8 103.0 1.8 111.0 1.6 129.0 1.4
400 MHz in D2O
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1H NMR 399.65 MHz C6 H13 N O3 0.035 g : 0.5 ml D2O 6-hydroxy-L-norleucine 
Assign. Shift(ppm)
A 3.746 B 3.624 C 1.89 D 1.603 E 1.45 THE SOLVENT PEAK SUPPRESSED.
Hz ppm Int.1503.30 3.762 194 1497.07 3.746 313 1490.97 3.731 188 1454.83 3.641 504 1448.49 3.625 1000 1441.89 3.608 491 764.04 1.912 168 762.57 1.909 172 762.33 1.908 172 758.79 1.899 175 755.00 1.890 219 753.66 1.886 222 748.05 1.872 195 746.70 1.869 176 746.22 1.868 177 648.32 1.623 288 641.36 1.605 482 634.40 1.588 404 627.69 1.571 152 586.67 1.468 151 584.23 1.462 143 577.51 1.446 220 573.12 1.435 138 570.19 1.427 191
in D2O
KBr disc
nujol mull
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