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MS-IW-0838 o-(1-pyrrolyl)aniline C10H10N2 (Mass of molecular ion: 158)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.0 28.0 2.1 31.0 1.1 39.0 3.4 41.0 1.1 50.0 1.0 51.0 2.7 52.0 2.3 53.0 1.0 63.0 1.6 64.0 1.6 65.0 6.7 66.0 4.5 77.0 4.4 78.0 3.4 79.0 4.1 91.0 1.8 92.0 3.1 102.0 1.2 103.0 3.9 104.0 2.7 117.0 1.4 118.0 2.8 119.0 1.0 128.0 1.2 129.0 3.2 130.0 33.1 131.0 14.8 132.0 5.5 143.0 1.0 155.0 2.4 156.0 11.6 157.0 86.2 158.0 100.0 159.0 11.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H10 N2 0.037 g : 0.5 ml CDCl3 o-(1-pyrrolyl)aniline Assign. Shift(ppm)
A 7.14 B 6.824 C 6.77 D 6.333 E 3.68
Hz ppm Int.
2865.11 7.170 133 2863.53 7.166 171 2857.54 7.151 207 2855.59 7.146 551 2853.88 7.141 200 2852.54 7.138 68 2849.98 7.132 134 2848.39 7.128 324 2847.17 7.125 410 2845.83 7.121 195 2729.49 6.830 623 2727.42 6.825 1000 2725.22 6.820 684 2715.09 6.794 111 2713.75 6.791 308 2712.28 6.787 389 2710.82 6.783 271 2706.91 6.774 301 2706.30 6.772 293 2705.44 6.770 204 2704.59 6.768 324 2702.88 6.764 249 2699.58 6.755 212 2698.24 6.752 128 2533.08 6.339 632 2531.01 6.334 956 2528.81 6.328 631 1471.68 3.683 130
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