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MassMS-NW-7056 tridecanophenone C19H30O (Mass of molecular ion: 274)
Source Temperature: 180 °C Sample Temperature: 120 °C Direct, 75 eV
27.0 6.2 28.0 1.3 29.0 12.5 39.0 3.5 41.0 18.5 42.0 4.0 43.0 16.6 50.0 1.1 51.0 6.3 53.0 1.1 55.0 9.8 56.0 2.5 57.0 5.1 67.0 1.0 69.0 2.7 71.0 1.1 76.0 1.2 77.0 29.5 78.0 5.5 79.0 1.1 91.0 2.2 105.0 62.5 106.0 5.1 107.0 1.0 120.0 100.0 121.0 11.4 133.0 10.0 134.0 1.5 274.0 7.8 275.0 2.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C19 H30 O 0.041 g : 0.5 ml CDCl3 tridecanophenone 
Assign. Shift(ppm)
A 7.95 B 7.49 C 2.96 D 1.72 E 1.26 F 0.878
Hz ppm Int.717.50 8.012 70 715.75 7.992 79 710.25 7.931 69 707.81 7.904 103 673.56 7.521 89 672.50 7.509 147 671.56 7.499 130 670.38 7.486 68 670.25 7.484 68 669.25 7.473 66 665.81 7.435 60 665.13 7.427 75 271.94 3.037 50 265.00 2.959 110 257.44 2.875 82 155.56 1.737 36 112.75 1.259 1000 84.56 0.945 54 83.56 0.934 59 83.25 0.930 56 82.94 0.927 56 82.25 0.919 56 81.50 0.911 55 80.75 0.902 58 78.75 0.880 155 76.63 0.856 49 75.25 0.841 37 74.94 0.837 37 74.44 0.832 37 74.13 0.828 35 73.69 0.823 38 72.69 0.812 46 71.88 0.803 39 71.56 0.800 38 71.00 0.793 31
in CDCl3
KBr disc
nujol mull
4880 A,200 M,powder
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