SpectrumDetail Supplier Related Products
WebSite > CAS DataBase List  > 6001-64-5More Spectrum  >1,1,1-TRICHLORO-2-METHYL-2-PROPANOL HEMIHYDRATE(6001-64-5)IR1

  • Mass

    MS-NW-1989          
    1,1,1-trichloro-2-methyl-2-propanol
    C4H7Cl3O (H2O)      (Mass of molecular ion:    176)
    

       Source Temperature: 240 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       5.0
          17.0       1.3
          18.0       4.9
          26.0       1.9
          27.0       7.2
          28.0       1.5
          29.0       2.1
          31.0      17.3
          36.0       1.4
          37.0       1.2
          38.0       1.2
          39.0       4.7
          41.0      15.7
          42.0       2.2
          43.0      27.2
          47.0       2.3
          49.0       1.5
          50.0       1.1
          51.0       2.1
          53.0       1.6
          55.0       1.0
          59.0     100.0
          60.0       3.5
          61.0       3.6
          62.0       2.0
          63.0       2.8
          77.0      15.2
          79.0       4.9
          82.0       2.0
          83.0       3.5
          84.0       1.4
          85.0       2.3
          87.0       1.1
          89.0       1.2
          91.0       1.0
          97.0       6.1
          99.0       4.0
         105.0       5.1
         107.0       1.6
         117.0       1.3
         119.0       1.1
         125.0      13.0
         126.0       2.2
         127.0       8.1
         128.0       1.2
         129.0       1.3
         161.0       5.1
         163.0       4.9
         165.0       1.5
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C4 H7 Cl3 O 0.048 g : 0.5 ml CDCl3
    1,1,1-trichloro-2-methyl-2-propanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.6 B 1.651

         Hz     ppm     Int.
    

        147.88   1.652   1000
        145.69   1.627     28
        145.13   1.621     21
    

in CDCl3



CCl4 solution



KBr disc



nujol mull



4880 A,200 M,powder