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MS-NW-0251 4-aminoazobenzene C12H11N3 (Mass of molecular ion: 197)
Source Temperature: 160 °C Sample Temperature: 0 °C Direct, 75 eV
18.0 1.9 28.0 1.9 38.0 1.9 39.0 9.2 41.0 2.4 50.0 1.9 51.0 9.8 52.0 3.6 53.0 1.5 54.0 1.3 62.0 1.1 63.0 3.8 64.0 3.2 65.0 28.8 66.0 4.0 77.0 22.2 78.0 2.9 79.0 1.4 91.0 3.1 92.0 100.0 93.0 10.7 98.5 1.1 105.0 1.7 115.0 1.7 120.0 33.9 121.0 2.9 141.0 1.6 167.0 3.3 168.0 2.3 169.0 1.1 196.0 1.2 197.0 70.6 198.0 10.4 199.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H11 N3 0.035 g : 0.5 ml CDCl3 4-aminoazobenzene Assign. Shift(ppm)
A 7.843 B 7.806 C 7.468 D 7.390 E 6.702 F 4.00
Hz ppm Int.
3141.11 7.860 173 3140.14 7.858 477 3138.79 7.854 638 3136.72 7.849 195 3132.45 7.838 297 3131.59 7.836 585 3130.86 7.835 478 3130.37 7.833 598 3128.17 7.828 126 3127.20 7.825 151 3124.39 7.818 912 3122.31 7.813 304 3120.00 7.807 70 3117.55 7.801 288 3115.48 7.796 1000 3112.67 7.789 123 2995.00 7.495 93 2993.90 7.492 205 2992.92 7.489 321 2991.21 7.485 153 2988.04 7.477 127 2985.72 7.471 629 2984.38 7.468 397 2979.49 7.456 212 2978.03 7.452 439 2977.42 7.451 372 2975.71 7.446 93 2960.69 7.409 166 2959.35 7.405 319 2958.01 7.402 190 2955.44 7.396 36 2954.10 7.392 129 2952.03 7.387 316 2949.83 7.382 105 2946.04 7.372 83 2944.82 7.369 138 2943.48 7.366 77 2685.67 6.721 127 2682.86 6.714 906 2680.66 6.708 294 2677.86 6.701 62 2676.03 6.696 280 2673.95 6.691 927 2671.14 6.684 112 1601.20 4.007 76
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