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MassMS-NW-7154 9-phenyl-9-xanthenol C19H14O2 (Mass of molecular ion: 274)
Source Temperature: 170 °C Sample Temperature: 130 °C Direct, 75 eV
18.0 3.0 39.0 1.8 50.0 1.4 51.0 4.3 63.0 1.9 65.0 1.3 75.0 1.4 76.0 1.2 77.0 6.5 88.0 1.0 92.0 1.1 100.0 1.5 101.0 1.3 113.0 2.7 115.0 4.8 121.0 1.6 127.5 1.5 128.0 1.7 137.0 1.7 139.0 3.2 141.0 3.4 152.0 1.5 168.0 2.6 181.0 3.8 196.0 3.5 197.0 100.0 198.0 14.5 199.0 1.7 202.0 1.1 226.0 2.3 227.0 1.0 228.0 1.4 243.0 1.2 255.0 5.8 256.0 2.1 257.0 13.7 258.0 4.2 274.0 8.2 275.0 1.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C19 H14 O2 0.038 g : 0.5 ml CDCl3 9-phenyl-9-xanthenol 
Assign. Shift(ppm)
A 7.385 B 7.340 C 7.28 D 7.26 E 7.18 F 7.17 G 7.042 J 2.66
Hz ppm Int.2956.30 7.398 466 2955.08 7.395 551 2953.00 7.389 147 2948.73 7.379 528 2947.88 7.377 770 2944.58 7.368 86 2938.11 7.352 572 2937.74 7.351 549 2936.52 7.348 594 2930.30 7.333 648 2928.71 7.329 666 2916.99 7.299 314 2916.26 7.298 192 2915.41 7.295 261 2909.79 7.281 844 2908.69 7.279 705 2908.20 7.277 602 2907.10 7.275 433 2902.59 7.263 962 2901.61 7.261 797 2900.02 7.257 473 2896.24 7.247 278 2894.78 7.244 410 2892.70 7.239 82 2890.87 7.234 448 2890.01 7.232 755 2872.31 7.188 1000 2871.46 7.185 802 2868.16 7.177 178 2866.58 7.173 405 2864.14 7.167 688 2863.16 7.165 513 2860.11 7.157 123 2858.89 7.154 144 2857.67 7.151 69 2821.17 7.060 514 2819.95 7.057 395 2817.14 7.050 43 2814.09 7.042 683 2813.35 7.040 692 2812.13 7.037 388 2810.18 7.032 42 2809.33 7.030 36 2808.72 7.028 37 2806.27 7.022 391 2804.93 7.019 300 1062.38 2.659 822
in CDCl3
KBr disc
nujol mull
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