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(+/-)-exo-6-Hydroxytropinone

Product Name (+/-)-exo-6-Hydroxytropinone

CAS5932-53-6

MFC8H13NO2

MW155.19

¹³CNMR

Mass

MS-NW-8076          
6-hydroxy-8-methyl-8-azabicyclo(3.2.1)octan-3-one
C8H13NO2            (Mass of molecular ion:    155)

   Source Temperature: 140 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      15.0       7.4
      18.0       2.2
      26.0       1.1
      27.0       7.5
      28.0      10.8
      29.0       5.2
      30.0       3.8
      31.0       2.0
      39.0       6.0
      40.0       1.5
      41.0      15.9
      42.0      77.0
      43.0       7.4
      44.0       5.9
      53.0       2.5
      54.0       5.5
      55.0      12.7
      56.0       9.0
      57.0      16.4
      58.0       9.7
      67.0       2.3
      68.0       5.0
      69.0       5.5
      70.0       6.5
      71.0       2.0
      72.0       3.2
      80.0       1.7
      81.0       2.7
      82.0      39.9
      83.0      85.3
      84.0       9.6
      86.0       1.3
      94.0       7.2
      95.0       1.5
      96.0      12.7
      97.0      21.7
      98.0      17.3
      99.0       1.2
     110.0      11.9
     111.0     100.0
     112.0      18.3
     113.0       2.0
     126.0       3.7
     138.0       3.3
     155.0      45.3
     156.0       5.8

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₃ N O₂	0.030 g : 0.5 ml CDCl₃
6-hydroxy-8-methyl-8-azabicyclo(3.2.1)octan-3-one

    Assign.     Shift(ppm)

      A             4.067
      B             3.597
      C             3.383
      D             3.1
      E             2.68
      F             2.655
      G     *1      2.206
      J     *1      2.095
      K             2.055
      L             1.994
     
     ASSIGNED BY C-H COSY

     Hz     ppm     Int.

   1630.49   4.080     69
   1627.93   4.074     74
   1623.54   4.063     74
   1620.85   4.056     71
   1441.53   3.607     34
   1437.99   3.599     45
   1436.65   3.595     47
   1435.06   3.591     38
   1432.62   3.585     36
   1431.27   3.582     32
   1354.74   3.390     68
   1349.61   3.377     70
   1085.33   2.716     38
   1080.69   2.705     85
   1075.32   2.691     56
   1071.17   2.681     38
   1069.21   2.676     43
   1064.33   2.664    116
   1061.04   2.655   1000
    891.24   2.231     47
    889.40   2.226     82
    887.57   2.221     49
    874.88   2.190     38
    873.17   2.185     70
    871.34   2.181     42
    848.02   2.122     48
    846.07   2.118     79
    844.12   2.113     42
    836.18   2.093     31
    832.28   2.083     45
    830.20   2.078     88
    828.25   2.073     57
    821.90   2.057     73
    814.82   2.039     70
    805.42   2.016     49
    803.34   2.011     31
    798.34   1.998     46

in CDCl3

KBr disc

nujol mull

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