8,8,10,10-Tetrakis(p-bromophenylsulfonyloxymethyl)-8,9,10,11-tetrahydro-7H-cycloocta[de]naphthalene

Assign. Shift(ppm) A *1 7.822 B *2 7.78 C 7.75 D *1 7.675 E *2 7.621 F 7.192 G 6.922 J *3 4.210 K *3 4.099 L 3.719 M *3 3.493 N *3 3.347 P 2.848 Q 1.395 R 0.537 J(J,K)=10.0HZ. J(L,P)=15.1HZ. J(Q,R)=15.2HZ. J(M,N)=9.4HZ.

     Hz     ppm     Int.

   3134.03   7.842     85
   3132.08   7.838    429
   3129.88   7.832    182
   3128.17   7.828     78
   3127.56   7.826     71
   3125.37   7.821    252
   3123.17   7.815   1000
   3121.22   7.810    213
   3118.90   7.805     62
   3118.53   7.804     61
   3116.94   7.800     58
   3112.79   7.789    221
   3110.84   7.784    983
   3108.64   7.779    271
   3106.45   7.773    102
   3104.13   7.768    212
   3101.93   7.762    535
   3099.98   7.757    280
   3096.68   7.749     71
   3096.44   7.748     71
   3095.58   7.746     76
   3092.65   7.739    260
   3091.67   7.736    232
   3088.75   7.729     49
   3088.38   7.728     47
   3087.89   7.727     46
   3087.16   7.725     41
   3086.55   7.724     42
   3085.94   7.722     41
   3085.69   7.721     41
   3084.84   7.719     42
   3078.61   7.704     49
   3077.76   7.702     55
   3075.44   7.696     90
   3073.36   7.691    466
   3071.29   7.685    194
   3069.21   7.680     89
   3068.60   7.679     90
   3068.36   7.678     90
   3066.65   7.674    257
   3064.45   7.668    951
   3062.50   7.663    191
   3060.06   7.657     53
   3059.33   7.656     53
   3058.72   7.654     50
   3058.11   7.652     54
   3057.62   7.651     52
   3056.88   7.649     50
   3056.52   7.648     49
   3055.66   7.646     49
   3054.81   7.644     46
   3053.71   7.641     67
   3052.98   7.640     64
   3050.90   7.634    194
   3048.83   7.629    929
   3046.75   7.624    258
   3042.11   7.612    185
   3040.04   7.607    475
   3037.96   7.602     74
   2881.96   7.212    172
   2877.08   7.200     43
   2874.88   7.194    223
   2873.78   7.191    207
   2866.70   7.174    180
   2770.26   6.932    189
   2769.17   6.929    197
   2766.72   6.923     47
   2766.24   6.922     44
   2765.63   6.921     47
   2763.18   6.915    169
   2762.08   6.912    166
   1688.48   4.225    172
   1678.47   4.200    243
   1642.33   4.110    241
   1639.04   4.102     41
   1632.32   4.085    173
   1494.38   3.740    133
   1482.67   3.710     41
   1479.25   3.702    142
   1476.56   3.695     53
   1401.25   3.507    194
   1391.97   3.483    250
   1341.80   3.358    241
   1332.40   3.334    199
   1145.51   2.867    145
   1130.37   2.829    137
    564.82   1.414     66
    564.58   1.413     66
    564.09   1.412     63
    563.60   1.411     57
    562.99   1.409     45
    549.80   1.376     71
    549.19   1.375     73
    222.05   0.556     92
    206.67   0.518     88