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3,5-Dichlorophenol

Product Name 3,5-Dichlorophenol

CAS591-35-5

MFC6H4Cl2O

MW163

¹³CNMR

Mass

MS-NW-1278          
3,5-dichlorophenol
C6H4Cl2O            (Mass of molecular ion:    162)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      28.0       1.4
      29.0       1.0
      31.0       1.6
      36.0       1.1
      37.0       3.8
      38.0       4.3
      39.0       2.9
      48.0       1.3
      49.0       5.0
      50.0       2.7
      53.0       3.3
      60.0       1.6
      61.0       5.2
      62.0       8.3
      63.0      24.6
      64.0       2.5
      72.0       1.1
      73.0      10.4
      74.0       2.5
      75.0       3.4
      81.0       3.7
      82.0       2.3
      83.0       1.0
      87.0       1.2
      91.0       1.6
      97.0       1.8
      98.0      11.7
      99.0      30.9
     100.0       5.5
     101.0      10.2
     126.0       3.8
     127.0       4.1
     128.0       1.7
     129.0       1.4
     133.0       3.3
     134.0       3.0
     135.0       2.3
     136.0       2.0
     162.0     100.0
     163.0       6.7
     164.0      63.7
     165.0       4.4
     166.0      10.6

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₆ H₄ Cl₂ O	0.052 g : 0.5 ml CDCl₃
3,5-dichlorophenol

    Assign.     Shift(ppm)

      A             6.946
      B             6.747
      C             5.15

     Hz     ppm     Int.

    624.00   6.968    192
    622.31   6.949    421
    620.50   6.929    285
    605.00   6.756   1000
    603.25   6.736    848
    601.69   6.719     50
    460.94   5.147    145

in CDCl3

CCl4 solution

KBr disc

nujol mull

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