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MassMS-IW-3633 n-(triphenylmethyl)glycine C21H19NO2 (Mass of molecular ion: 317)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
18.0 1.8 28.0 1.7 30.0 3.9 39.0 1.2 44.0 2.0 51.0 2.4 63.0 1.3 65.0 1.5 75.0 1.0 77.0 6.0 89.0 1.2 91.0 37.1 92.0 2.8 94.5 1.5 101.0 1.7 104.0 9.8 105.0 3.1 106.5 1.6 107.5 2.2 113.0 2.5 114.0 1.5 115.0 3.1 116.0 1.7 118.5 1.2 119.0 1.5 119.5 3.9 120.0 2.5 120.5 1.0 121.5 1.3 139.0 2.0 152.0 2.7 154.0 1.1 163.0 3.6 164.0 3.2 165.0 50.3 166.0 10.7 167.0 8.0 168.0 1.0 180.0 2.0 182.0 4.0 183.0 1.6 189.0 1.1 194.0 3.8 202.0 2.3 213.0 1.2 215.0 4.2 216.0 1.0 226.0 2.6 227.0 1.8 228.0 6.2 229.0 1.7 237.0 1.1 239.0 8.3 240.0 100.0 241.0 27.3 242.0 11.4 243.0 79.9 244.0 27.1 245.0 3.8 257.0 1.1 258.0 13.4 259.0 3.0 317.0 6.6 318.0 1.5
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C21 H19 N O2 0.050 g : 0.5 ml DMSO-d6 N-(triphenylmethyl)glycine 
Assign. Shift(ppm)
A 7.412 B 7.307 C 7.211 D 3.6 E 2.894
Hz ppm Int.2968.26 7.428 568 2966.92 7.424 760 2959.72 7.406 1000 2958.74 7.404 949 2948.00 7.377 30 2928.47 7.328 590 2926.64 7.324 223 2921.02 7.309 994 2913.09 7.290 597 2888.06 7.227 390 2886.84 7.224 260 2882.69 7.214 181 2880.74 7.209 534 2878.78 7.204 178 2874.63 7.193 130 2873.54 7.191 204 2872.31 7.188 126 1156.86 2.895 743
in DMSO-d6
KBr disc
nujol mull
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