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3-Phenoxypropyl bromide

Product Name 3-Phenoxypropyl bromide

CAS588-63-6

MFC9H11BrO

MW215.09

¹³CNMR

Mass

MS-NW-5681          
3-bromopropyl phenyl ether
C9H11BrO            (Mass of molecular ion:    214)

   Source Temperature: 270 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       2.2
      28.0       1.6
      38.0       1.7
      39.0       9.7
      40.0       1.9
      41.0      18.7
      42.0       1.5
      50.0       2.1
      51.0       6.1
      55.0       1.2
      63.0       2.3
      64.0       1.2
      65.0       7.8
      66.0       7.4
      77.0      12.4
      78.0       1.9
      79.0       1.9
      91.0       1.1
      94.0     100.0
      95.0       7.8
     107.0       4.5
     121.0       4.4
     123.0       4.1
     134.0       1.4
     135.0       5.5
     214.0      16.5
     215.0       1.9
     216.0      16.5
     217.0       1.9

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₉ H₁₁ Br O	0.04 ml : 0.5 ml CDCl₃
3-bromopropyl phenyl ether

    Assign.     Shift(ppm)

      A             7.27
      B             6.94
      C             6.90
      D             4.089
      E             3.585
      F             2.307

     Hz     ppm     Int.

    661.06   7.382    166
    660.00   7.370    173
    658.13   7.349    111
    654.56   7.309    127
    653.88   7.302    230
    652.50   7.286    381
    650.63   7.265    161
    647.56   7.231    217
    647.19   7.227    191
    645.44   7.207    369
    645.06   7.203    396
    644.31   7.195    370
    629.88   7.034    104
    628.88   7.022    164
    628.38   7.017    209
    627.38   7.006    271
    624.19   6.970    146
    622.06   6.946    880
    621.00   6.934    414
    620.00   6.923    394
    615.31   6.871    205
    613.69   6.853    395
    612.75   6.842    318
    372.31   4.158    496
    366.50   4.093    973
    360.69   4.028    547
    328.19   3.665    403
    321.69   3.592   1000
    315.38   3.522    614
    218.69   2.442    109
    218.13   2.436    126
    212.63   2.375    364
    212.13   2.369    365
    206.13   2.302    476
    200.13   2.235    302

in CDCl3

liquid film

4880 A,200 M,liquid

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