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MassMS-IW-9044 tributyl orthoformate C13H28O3 (Mass of molecular ion: 232)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 1.1 26.0 1.4 27.0 10.1 28.0 8.5 29.0 17.8 31.0 14.0 39.0 8.2 40.0 1.9 41.0 42.4 42.0 5.1 43.0 9.5 44.0 1.2 45.0 1.7 47.0 2.4 50.0 1.0 53.0 1.6 55.0 9.4 56.0 36.5 57.0 100.0 58.0 4.4 73.0 2.2 103.0 29.8 104.0 1.7 159.0 28.8 160.0 2.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H28 O3 0.05 ml : 0.5 ml CDCl3 tributyl orthoformate 
Assign. Shift(ppm)
A 5.136 B 3.534 C 1.586 D 1.400 E 0.926
Hz ppm Int.2052.86 5.137 302 1419.19 3.552 382 1412.48 3.535 682 1405.88 3.518 384 647.34 1.620 74 640.87 1.604 200 640.14 1.602 208 637.57 1.596 81 633.54 1.586 254 630.86 1.579 164 625.61 1.566 231 619.02 1.549 113 578.25 1.447 60 572.75 1.434 50 570.80 1.429 180 565.31 1.415 119 563.11 1.410 247 557.86 1.396 122 555.54 1.391 252 550.66 1.378 61 548.22 1.372 162 541.02 1.354 53 377.32 0.945 605 369.87 0.926 1000 362.55 0.908 531
in CDCl3
liquid film
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