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2-(Hydroxymethyl)pyridine

Product Name 2-(Hydroxymethyl)pyridine

CAS586-98-1

MFC6H7NO

MW109.13

¹³CNMR

Mass

MS-NW-3076          
2-pyridinemethanol
C6H7NO              (Mass of molecular ion:    109)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      18.0       1.2
      26.0       3.7
      27.0       8.9
      28.0       4.4
      29.0       3.9
      31.0       5.8
      37.0       2.0
      38.0       3.5
      39.0       8.7
      40.0       1.1
      41.0       1.0
      49.0       1.7
      50.0       8.8
      51.0      21.4
      52.0      29.3
      53.0      21.7
      54.0       1.8
      62.0       1.2
      63.0       2.8
      64.0       3.1
      65.0       4.8
      75.0       1.0
      76.0       1.3
      78.0      32.4
      79.0      32.9
      80.0      58.3
      81.0       4.2
      91.0       1.0
      92.0       2.0
     106.0       2.6
     107.0       1.1
     108.0     100.0
     109.0      54.4
     110.0       3.8

400 MHz in CDCl3

90 MHz in CDCl3

parameter in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₇ N O	0.05 ml : 0.5 ml CDCl₃
2-pyridinemethanol

    Assign.     Shift(ppm)

      A             8.454
      B             7.653
      C             7.374
      D             7.147
      E             5.4
      F             4.750

     Hz     ppm     Int.

   3382.69   8.465    137
   3381.84   8.463    163
   3380.98   8.460    173
   3380.00   8.458    159
   3377.81   8.452    145
   3376.83   8.450    164
   3376.10   8.448    170
   3375.12   8.446    155
   3067.63   7.676    142
   3065.80   7.672    148
   3059.81   7.657    247
   3057.98   7.652    244
   3052.25   7.638    170
   3050.42   7.633    166
   2951.54   7.386    176
   2950.44   7.383    238
   2949.46   7.381    183
   2944.34   7.368     76
   2943.73   7.366    152
   2942.75   7.364    207
   2941.53   7.361    156
   2863.65   7.166     81
   2863.04   7.164    147
   2862.43   7.163    145
   2861.82   7.161    151
   2861.21   7.160     93
   2858.03   7.152    141
   2857.42   7.150    141
   2856.81   7.149    146
   2856.20   7.147    130
   2855.47   7.145    148
   2854.86   7.144    137
   2854.25   7.142    136
   2853.64   7.141     82
   2851.20   7.135     69
   2850.59   7.133    128
   2849.98   7.132    123
   2849.37   7.130    127
   2848.75   7.129     73
   1898.19   4.750   1000

¹H NMR	89.56 MHz
C₆ H₇ N O	0.04 ml : 0.5 ml CDCl₃
2-pyridinemethanol

    Assign.     Shift(ppm)

      A             8.49
      B             7.65
      C             7.34
      D             7.17
      E             4.85
      F             4.752

     Hz     ppm     Int.

    764.25   8.534    102
    763.19   8.522    125
    762.50   8.514    129
    761.63   8.505    111
    759.31   8.479    116
    758.38   8.468    136
    757.63   8.460    135
    756.69   8.449    114
    695.56   7.767     76
    693.75   7.747     77
    688.13   7.684    158
    686.25   7.663    158
    680.38   7.597    172
    678.56   7.577    166
    659.81   7.368    210
    653.31   7.295     96
    652.38   7.285    124
    651.94   7.280    119
    648.06   7.237    124
    647.44   7.230    103
    646.75   7.222     98
    643.19   7.182    112
    642.50   7.174     96
    641.81   7.167    107
    641.31   7.161    100
    640.75   7.155     97
    640.06   7.147     82
    639.38   7.140     79
    635.81   7.100     78
    635.19   7.093     71
    634.50   7.085     68
    434.50   4.852    108
    425.56   4.752   1000

¹H NMR	300 MHz
C₆ H₇ N O	30 % in DMSO
2-pyridinemethanol

    Parameter     ppm  Hz

      D(A)         8.65
      D(B)         7.40
      D(C)         8.05
      D(D)         7.75
       J(A,B)          4.6
       J(A,C)          2.0
       J(A,D)          1.2
       J(B,C)          7.8
       J(B,D)          1.0
       J(C,D)          8.0
     
      D(E)         4.81
     
      D(F)         5.60
     
     BRUEGEL,W. Z.ELEKTROCHEM.BER.BUNSENGES.PHYS.CHEM.
     66, 159 (1962)

     Hz     ppm     Int.

   2598.89   8.663     51
   2597.67   8.659     64
   2596.99   8.657     65
   2595.74   8.652     59
   2594.31   8.648     59
   2593.10   8.644     66
   2592.38   8.641     65
   2591.20   8.637     54
   2424.13   8.080     40
   2422.17   8.074     39
   2416.27   8.054     86
   2414.30   8.048     84
   2408.36   8.028     52
   2406.39   8.021     50
   2329.85   7.766     65
   2328.85   7.763    104
   2327.81   7.759     65
   2321.88   7.740     54
   2320.84   7.736     87
   2319.84   7.733     55
   2226.56   7.422     55
   2225.67   7.419     54
   2221.98   7.407     55
   2221.02   7.403     55
   2218.83   7.396     53
   2217.87   7.393     51
   2214.18   7.381     50
   2213.29   7.378     49
   1680.01   5.600   1000
   1442.98   4.810    667

in CDCl3

liquid film

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