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MassMS-NW-8815 2,6-di-tert-butylpyridine C13H21N (Mass of molecular ion: 191)
Source Temperature: 270 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.5 29.0 3.4 39.0 3.1 41.0 6.6 51.0 1.9 52.0 1.2 53.0 1.9 57.0 1.6 65.0 3.2 65.5 2.5 66.0 1.7 66.5 1.9 67.0 1.0 77.0 4.8 78.0 2.7 79.0 2.5 80.0 1.6 80.5 1.3 91.0 6.2 92.0 2.2 93.0 3.0 104.0 2.4 105.0 1.3 106.0 1.0 107.0 1.1 117.0 3.7 118.0 4.8 119.0 2.5 120.0 4.9 121.0 1.5 130.0 1.2 132.0 1.6 133.0 4.1 134.0 4.4 135.0 21.2 136.0 3.9 144.0 2.9 146.0 6.9 147.0 1.8 149.0 59.3 150.0 6.8 158.0 2.9 159.0 1.1 160.0 21.9 161.0 19.2 162.0 2.9 174.0 9.1 175.0 7.7 176.0 100.0 177.0 13.8 190.0 52.4 191.0 33.9 192.0 4.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C13 H21 N 0.05 ml : 0.5 ml CDCl3 2,6-di-tert-butylpyridine 
Assign. Shift(ppm)
A 7.468 B 7.070 C 1.345
Hz ppm Int.662.44 7.397 26 636.50 7.107 55 636.00 7.102 52 629.06 7.024 34 627.94 7.012 30 120.50 1.346 1000
in CDCl3
liquid film
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