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MS-IW-1793 1-phenyl-1-pentanol C11H16O (Mass of molecular ion: 164)
Source Temperature: 230 °C Sample Temperature: 160 °C Reservoir, 75 eV
27.0 1.5 29.0 1.5 39.0 1.7 41.0 1.8 51.0 3.4 57.0 1.1 77.0 14.8 78.0 3.5 79.0 34.3 80.0 2.3 91.0 2.8 103.0 1.1 104.0 1.5 105.0 6.9 106.0 1.1 107.0 100.0 108.0 8.2 115.0 1.2 117.0 2.6 120.0 1.6 163.0 2.0 164.0 6.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H16 O 0.05 ml : 0.5 ml CDCl3 1-phenyl-1-pentanol Assign. Shift(ppm)
A 7.30 B 7.28 C 7.22 D 4.550 E 2.6 F *1 1.73 G *1 1.64 J *2 1.33 K 1.29 L *2 1.19 M 0.861
Hz ppm Int.
2924.80 7.319 89 2923.58 7.316 124 2922.00 7.312 67 2921.02 7.309 43 2918.09 7.302 201 2916.26 7.298 435 2915.16 7.295 391 2912.96 7.289 149 2911.13 7.285 600 2910.64 7.283 624 2909.42 7.280 959 2908.33 7.278 843 2903.93 7.267 140 2902.34 7.263 216 2900.02 7.257 80 2895.39 7.245 179 2893.43 7.240 167 2892.46 7.238 132 2889.89 7.232 146 2888.67 7.229 102 2886.72 7.224 188 2885.62 7.221 113 2883.30 7.215 113 2880.49 7.208 95 2879.03 7.204 156 2878.17 7.202 65 1825.44 4.568 164 1819.34 4.553 205 1818.12 4.550 206 1812.01 4.534 171 1045.65 2.617 34 1037.35 2.596 33 707.03 1.770 31 701.66 1.756 57 699.58 1.751 45 698.61 1.749 61 696.90 1.744 62 694.21 1.738 69 693.60 1.736 76 691.16 1.730 62 689.45 1.726 68 688.35 1.723 116 686.16 1.717 72 683.35 1.710 82 680.91 1.704 107 675.90 1.692 77 672.12 1.682 44 666.38 1.668 108 661.99 1.657 69 660.40 1.653 91 658.69 1.649 49 656.49 1.643 100 652.95 1.634 65 650.51 1.628 90 648.32 1.623 47 646.97 1.619 50 643.07 1.610 56 637.08 1.595 41 548.95 1.374 46 543.95 1.362 53 541.75 1.356 53 540.16 1.352 37 538.94 1.349 45 536.62 1.343 53 535.28 1.340 64 531.37 1.330 109 530.03 1.327 105 526.00 1.317 175 525.02 1.314 188 521.85 1.306 124 519.90 1.301 286 512.82 1.284 347 505.86 1.266 235 499.15 1.249 76 493.77 1.236 42 493.04 1.234 38 489.38 1.225 52 487.79 1.221 41 486.45 1.218 41 483.89 1.211 83 483.15 1.209 82 480.59 1.203 40 479.00 1.199 56 477.54 1.195 70 475.22 1.190 70 473.51 1.185 58 472.78 1.183 61 470.21 1.177 64 467.16 1.169 52 465.09 1.164 61 459.59 1.150 32 351.07 0.879 525 344.12 0.862 1000 339.97 0.851 111 338.62 0.848 142 336.79 0.843 437
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