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58230-69-6More Spectrum > N-(4-AMINO-2-METHYLPHENYL)-4-CHLOROPHTHALIMIDE(58230-69-6)13CNMR
N-(4-AMINO-2-METHYLPHENYL)-4-CHLOROPHTHALIMIDE
Product Name N-(4-AMINO-2-METHYLPHENYL)-4-CHLOROPHTHALIMIDE
CAS58230-69-6
MFC15H11ClN2O2
MW286.71
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MS-IW-0845 N-(4-amino-2-methylphenyl)-4-chlorophthalimide C15H11ClN2O2 (Mass of molecular ion: 286)
Source Temperature: 180 °C Sample Temperature: 160 °C Direct, 75 eV
65.0 1.0 75.0 2.4 77.0 2.3 78.0 1.8 79.0 1.2 93.0 1.0 102.5 1.2 103.0 1.9 104.0 5.1 105.0 3.0 106.0 1.9 110.0 3.2 111.0 1.2 112.0 1.1 119.0 2.0 120.0 2.0 134.0 1.6 135.5 1.2 138.0 2.0 139.0 1.2 143.0 3.2 144.0 1.0 164.0 1.8 167.0 1.1 180.0 3.1 194.0 1.0 195.0 1.0 205.0 3.7 206.0 2.6 207.0 4.2 214.0 1.3 229.0 1.1 239.0 1.3 241.0 5.4 242.0 14.9 243.0 4.0 244.0 4.9 257.0 1.5 268.0 48.2 269.0 15.8 270.0 17.5 271.0 5.2 285.0 2.2 286.0 100.0 287.0 18.0 288.0 33.5 289.0 5.7
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C15 H11 Cl N2 O2 0.034 g : 0.5 ml DMSO-d6 N-(4-amino-2-methylphenyl)-4-chlorophthalimide Assign. Shift(ppm)
A 8.015 B 7.95 C 7.94 D 6.923 E 6.533 F 6.484 G 5.33 J 1.946
Hz ppm Int.
3204.47 8.019 238 3203.61 8.017 318 3203.00 8.015 287 3202.03 8.013 263 3185.30 7.971 32 3184.33 7.968 45 3177.25 7.951 486 3176.39 7.948 727 3174.80 7.944 369 3168.33 7.928 37 3166.75 7.924 42 2771.36 6.935 226 2762.94 6.914 251 2612.30 6.537 164 2609.99 6.531 204 2596.68 6.498 129 2594.12 6.491 99 2588.26 6.477 115 2585.82 6.471 97 2130.74 5.332 368 2123.29 5.313 37 777.71 1.946 1000
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