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2,3'-Bipyridine

Product Name 2,3'-Bipyridine

CAS581-50-0

MFC10H8N2

MW156.18

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  • Mass 

    MS-NW-7293          
2,3'-bipyridine
C10H8N2             (Mass of molecular ion:    156)


       Source Temperature: 200 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          26.0       1.1
      27.0       1.2
      38.0       1.2
      39.0       2.0
      50.0       7.6
      51.0      11.9
      52.0       5.8
      53.0       1.0
      62.0       1.4
      63.0       2.1
      64.0       2.3
      64.5       2.9
      65.0       1.1
      74.0       2.9
      75.0       4.2
      76.0       5.2
      77.0       4.3
      78.0      16.5
      79.0      10.3
     101.0       3.1
     102.0       3.3
     103.0       2.4
     104.0       9.8
     105.0       1.2
     128.0      10.3
     129.0       6.4
     130.0      21.9
     131.0       2.4
     155.0      68.7
     156.0     100.0
     157.0      11.6

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H8 N2 0.05 ml : 0.5 ml CDCl3
    2,3'-bipyridine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             9.208
      B             8.686
      C             8.628
      D             8.287
      E             7.726
      F             7.702
      G             7.361
      J             7.240
  

         Hz     ppm     Int.


       3681.49   9.212    668
   3680.88   9.211    679
   3679.35   9.207    661
   3475.49   8.697    497
   3474.43   8.694    542
   3473.66   8.692    557
   3472.75   8.690    471
   3470.61   8.685    499
   3469.54   8.682    555
   3468.93   8.680    566
   3467.86   8.678    454
   3451.69   8.637    516
   3450.01   8.633    523
   3446.81   8.625    528
   3445.28   8.621    502
   3318.02   8.303    483
   3316.35   8.299    558
   3315.73   8.297    526
   3314.06   8.293    444
   3310.09   8.283    500
   3308.41   8.279    557
   3307.80   8.277    541
   3306.12   8.273    434
   3098.60   7.754    272
   3096.77   7.749    242
   3091.58   7.736    310
   3090.67   7.734    715
   3089.90   7.732    346
   3088.84   7.729    663
   3083.65   7.716    847
   3081.97   7.712   1000
   3081.36   7.711    874
   3080.29   7.708    895
   3079.68   7.706    931
   3078.61   7.704    791
   3073.27   7.690    302
   3072.36   7.688    325
   3071.75   7.687    242
   3070.68   7.684    172
   2948.61   7.378    482
   2947.85   7.377    472
   2943.88   7.367    501
   2942.96   7.364    482
   2940.67   7.359    488
   2939.91   7.357    449
   2935.94   7.347    455
   2935.03   7.345    450
   2900.24   7.257    488
   2898.56   7.253    458
   2895.36   7.245    493
   2893.68   7.241    584
   2893.22   7.240    596
   2891.54   7.236    458
   2888.49   7.228    464
   2886.81   7.224    412

in CDCl3



liquid film



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