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MassMS-NW-0085 dodecahydrofluorene C13H22 (Mass of molecular ion: 178)
Source Temperature: 240 °C Sample Temperature: 95 °C Reservoir, 75 eV
18.0 1.2 27.0 5.9 28.0 5.8 29.0 6.2 39.0 10.2 40.0 1.7 41.0 25.0 42.0 1.9 43.0 2.2 51.0 2.0 52.0 1.2 53.0 8.9 54.0 15.3 55.0 27.9 56.0 1.5 57.0 1.0 65.0 4.0 66.0 3.9 67.0 56.5 68.0 15.0 69.0 4.4 77.0 7.4 78.0 1.9 79.0 16.4 80.0 10.5 81.0 54.8 82.0 42.0 83.0 7.9 91.0 6.9 92.0 1.5 93.0 8.4 94.0 5.8 95.0 13.0 96.0 87.6 97.0 100.0 98.0 7.7 105.0 1.3 107.0 2.7 108.0 1.7 109.0 3.0 110.0 1.5 120.0 1.6 121.0 16.5 122.0 2.8 135.0 5.6 136.0 1.9 149.0 1.8 150.0 1.9 178.0 25.4 179.0 3.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H22 0.04 ml : 0.5 ml CDCl3 dodecahydrofluorene 
Assign. Shift(ppm)
A 1.94 B 1.84 C 1.73 D 1.63 E 1.55 F 1.46 G 1.35 J 1.22 NOT ASSIGNED
Hz ppm Int.745.61 1.866 377 739.62 1.851 438 738.16 1.848 358 735.96 1.842 346 733.64 1.836 368 732.30 1.833 390 696.90 1.744 431 692.38 1.733 346 684.33 1.713 514 655.03 1.640 391 652.59 1.633 499 647.34 1.620 625 645.26 1.615 458 642.33 1.608 388 639.28 1.600 377 629.88 1.577 336 629.03 1.574 331 627.44 1.570 379 623.90 1.562 386 623.29 1.560 359 621.58 1.556 356 616.33 1.543 361 615.23 1.540 409 611.82 1.531 377 610.84 1.529 375 609.50 1.526 379 594.24 1.487 643 593.63 1.486 643 589.23 1.475 558 588.26 1.472 543 586.30 1.468 661 584.96 1.464 647 583.50 1.461 578 582.64 1.458 605 581.42 1.455 639 580.44 1.453 674 577.64 1.446 778 575.56 1.441 438 573.61 1.436 418 572.51 1.433 360 568.85 1.424 408 566.28 1.417 353 558.84 1.399 569 555.18 1.390 470 554.32 1.388 480 550.42 1.378 510 548.71 1.373 575 547.73 1.371 750 546.63 1.368 909 545.04 1.364 749 542.48 1.358 752 541.75 1.356 729 539.55 1.351 1000 538.33 1.348 939 536.13 1.342 697 535.03 1.339 623 530.15 1.327 674 527.95 1.322 792 526.61 1.318 701 525.76 1.316 562 523.07 1.309 426 517.46 1.295 385 515.50 1.290 492 492.07 1.232 335 488.28 1.222 382 486.45 1.218 345 484.86 1.214 435
in CDCl3
liquid film
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