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MS-NW-4033 1,4-naphthalenediol C10H8O2 (Mass of molecular ion: 160)
Source Temperature: 190 °C Sample Temperature: 110 °C Direct, 75 eV
17.0 1.4 18.0 6.2 27.0 1.8 28.0 1.2 38.0 1.5 39.0 1.8 50.0 6.0 51.0 7.2 52.0 1.8 53.0 2.1 54.0 1.1 55.0 1.8 62.0 1.1 63.0 2.1 65.5 1.7 66.0 3.0 74.0 3.1 75.0 3.4 76.0 10.5 77.0 15.0 78.0 2.9 80.0 2.9 82.0 1.5 102.0 5.5 103.0 11.4 104.0 19.2 105.0 16.3 106.0 1.4 114.0 1.0 115.0 2.8 130.0 2.7 131.0 35.7 132.0 14.5 133.0 1.7 158.0 5.1 159.0 6.6 160.0 100.0 161.0 11.2 162.0 1.1
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H8 O2 0.038 g : 0.5 ml DMSO-d6 1,4-naphthalenediol Assign. Shift(ppm)
A 9.326 B 8.076 C 7.431 D 6.703
Hz ppm Int.
3727.87 9.328 790 3237.15 8.100 42 3235.93 8.097 53 3233.18 8.091 292 3229.98 8.083 261 3227.08 8.075 265 3223.88 8.067 305 3223.42 8.066 320 3221.13 8.060 58 3219.91 8.057 42 2977.45 7.451 57 2974.70 7.444 294 2971.50 7.436 252 2968.29 7.428 247 2964.94 7.419 278 2962.49 7.413 56 2678.99 6.704 1000
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