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MS-IW-7203 4-ethylbiphenyl C14H14 (Mass of molecular ion: 182)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
39.0 1.2 51.0 1.7 63.0 2.0 64.0 1.0 69.5 1.0 70.5 1.3 75.0 1.0 76.0 4.7 77.0 3.5 82.0 2.8 82.5 4.3 83.0 3.3 83.5 7.2 84.0 1.0 88.0 1.0 89.0 3.2 90.0 1.5 91.0 3.9 115.0 3.1 127.0 1.0 128.0 2.1 139.0 1.6 141.0 1.3 151.0 2.2 152.0 11.3 153.0 2.8 154.0 1.2 164.0 1.6 165.0 19.5 166.0 7.4 167.0 100.0 168.0 14.2 178.0 2.9 179.0 2.0 180.0 2.1 181.0 5.0 182.0 60.0 183.0 9.1 210.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C14 H14 0.041 g : 0.5 ml CDCl3 4-ethylbiphenyl Assign. Shift(ppm)
A 7.568 B 7.508 C 7.404 D 7.305 E 7.260 F 2.678 G 1.264
Hz ppm Int.
3030.52 7.583 204 3029.17 7.580 242 3027.22 7.575 72 3023.93 7.567 92 3023.19 7.565 128 3022.09 7.562 274 3020.87 7.559 243 3018.92 7.554 36 3007.08 7.525 46 3005.00 7.520 282 3003.05 7.515 102 2998.66 7.504 115 2996.70 7.499 340 2994.63 7.494 48 2968.63 7.429 43 2967.65 7.426 105 2966.92 7.424 153 2965.09 7.420 61 2961.55 7.411 59 2960.94 7.409 78 2959.59 7.406 289 2958.37 7.403 129 2953.37 7.390 84 2951.78 7.386 162 2949.83 7.382 30 2926.88 7.324 70 2925.66 7.321 126 2924.32 7.318 72 2920.17 7.307 57 2918.21 7.302 136 2916.26 7.298 46 2912.11 7.287 41 2910.89 7.284 70 2909.67 7.281 42 2907.23 7.275 51 2905.27 7.270 280 2904.66 7.269 241 2903.20 7.265 93 2898.80 7.254 88 2897.34 7.250 207 2896.73 7.249 248 2894.78 7.244 34 1082.03 2.708 72 1074.46 2.689 216 1066.77 2.670 225 1059.20 2.651 79 513.06 1.284 482 505.37 1.265 1000 503.05 1.259 32 497.80 1.246 495
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