2,3-DICHLOROBENZAL CHLORIDE

Mass

MS-IW-2212          
alpha,alpha,2,3-tetrachlorotoluene
C7H4Cl4             (Mass of molecular ion:    228)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      36.0       1.7
      37.0       1.3
      38.0       1.2
      39.0       1.6
      43.0       3.0
      49.0       1.3
      50.0       2.1
      60.0       2.3
      60.5       1.3
      61.0       8.0
      62.0       6.1
      63.0       3.7
      72.0       1.2
      73.0       8.4
      74.0       1.7
      75.0       3.2
      78.0       2.4
      78.5       3.1
      79.0       3.3
      79.5       2.1
      80.0       1.4
      83.0       1.1
      84.0       1.7
      85.0       2.6
      86.0       3.6
      87.0       4.6
      88.0       1.2
      96.0       2.9
      96.5       5.9
      97.0       6.5
      97.5       5.6
      98.0       1.6
      98.5       1.8
      99.0       1.9
     107.0       2.2
     109.0       1.9
     123.0      15.4
     124.0       1.3
     125.0       4.9
     133.0       3.7
     135.0       2.2
     157.0       7.7
     158.0       5.0
     159.0       5.8
     160.0       3.2
     161.0       1.3
     167.0       1.0
     192.0       1.5
     193.0     100.0
     194.0       9.3
     195.0      96.2
     196.0       8.0
     197.0      31.5
     198.0       2.5
     199.0       3.4
     228.0      13.7
     229.0       1.3
     230.0      17.4
     231.0       1.5
     232.0       8.4
     234.0       1.8

Assign. Shift(ppm) A 7.848 B 7.462 C 7.295 D 7.153

     Hz     ppm     Int.

   3141.36   7.861    352
   3139.89   7.857    345
   3133.42   7.841    383
   3131.84   7.837    363
   2987.43   7.476    350
   2985.96   7.472    335
   2983.76   7.466     23
   2979.37   7.455    437
   2977.91   7.452    408
   2922.85   7.314    371
   2914.79   7.294    610
   2906.86   7.274    284
   2858.64   7.153   1000