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MassMS-NW-5122 1,1-dichloropropene C3H4Cl2 (Mass of molecular ion: 110)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.2 25.0 1.1 26.0 2.9 27.0 5.9 35.0 1.8 36.0 3.7 37.0 9.4 38.0 10.0 39.0 55.2 40.0 2.4 41.0 1.4 47.0 4.5 48.0 1.3 49.0 12.6 51.0 3.8 60.0 2.0 61.0 1.6 62.0 1.7 63.0 2.7 72.0 2.4 73.0 9.2 74.0 5.0 75.0 100.0 76.0 4.8 77.0 32.2 78.0 1.2 81.0 1.4 82.0 2.9 83.0 7.4 84.0 1.9 85.0 5.2 109.0 8.2 110.0 38.9 111.0 6.2 112.0 24.6 113.0 1.8 114.0 4.1
parameter in CDCl3
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1H NMR 300 MHz C3 H4 Cl2 0.04 ml : 0.5 ml CDCl3 1,1-dichloropropene 
Parameter ppm Hz
D(A) 5.892 D(B) 1.753 J(A,B) 6.9
Hz ppm Int.1777.97 5.927 82 1771.10 5.904 248 1764.19 5.881 249 1757.32 5.858 85 529.34 1.764 1000 522.47 1.742 989
in CDCl3
liquid film
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