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MS-NW-0415 titanium tetrabutoxide C16H36O4Ti (Mass of molecular ion: 340)
Source Temperature: 210 °C Sample Temperature: 280 °C Direct, 75 eV
15.0 1.8 17.0 1.2 18.0 6.4 26.0 5.8 27.0 34.7 28.0 21.3 29.0 31.3 30.0 1.1 31.0 31.3 32.0 1.4 33.0 3.1 37.0 2.0 38.0 3.2 39.0 26.8 40.0 5.7 41.0 100.0 42.0 23.8 43.0 73.9 44.0 10.0 45.0 3.7 50.0 3.3 51.0 3.3 52.0 1.3 53.0 6.5 54.0 6.4 55.0 38.7 56.0 95.6 57.0 39.0 58.0 5.0 60.0 3.7 61.0 2.6 66.0 1.0 67.0 10.4 68.0 6.5 69.0 17.9 70.0 6.5 71.0 9.2 72.0 6.6 73.0 4.4 74.0 1.1 77.0 1.4 79.0 3.4 80.0 2.6 81.0 10.1 82.0 7.3 83.0 12.4 84.0 7.0 85.0 5.8 87.0 2.4 91.0 2.2 93.0 3.1 94.0 1.9 95.0 7.3 96.0 6.0 97.0 9.2 98.0 12.4 99.0 2.3 101.0 2.1 105.0 2.0 107.0 1.9 108.0 1.4 109.0 4.2 110.0 3.0 111.0 5.6 112.0 3.5 113.0 1.2 115.0 1.3 116.0 3.1 117.0 2.0 119.0 1.2 121.0 2.0 122.0 1.0 123.0 2.8 124.0 2.0 125.0 2.5 126.0 1.2 127.0 1.0 129.0 4.1 133.0 1.0 135.0 2.0 136.0 1.1 137.0 2.3 138.0 1.9 139.0 1.5 143.0 1.2 145.0 1.0 147.0 1.2 149.0 1.2 151.0 1.3 152.0 1.9 153.0 1.3 157.0 1.1 165.0 1.8 166.0 1.1 167.0 1.1 180.0 1.0 185.0 1.7 193.0 1.1 194.0 2.0 208.0 1.1 211.0 1.1 222.0 1.1 224.0 1.6 225.0 2.9 229.0 1.6 236.0 3.0 237.0 1.5 239.0 1.6 241.0 1.0 243.0 1.5 255.0 1.5 256.0 1.1 257.0 2.9 264.0 1.3 265.0 2.4 266.0 2.2 267.0 14.7 268.0 3.7 269.0 1.7 295.0 2.5 296.0 2.8 297.0 22.1 298.0 5.0 299.0 2.4 368.0 1.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C16 H36 O4 Ti 0.04 ml : 0.5 ml CDCl3 titanium tetrabutoxide Assign. Shift(ppm)
A 4.16 B 1.58 C 1.37 D 0.93
Hz ppm Int.
372.75 4.163 298 366.94 4.098 193 157.56 1.760 47 151.13 1.688 145 149.25 1.667 140 144.56 1.615 286 138.31 1.545 359 132.44 1.479 359 126.63 1.414 312 124.50 1.391 370 121.13 1.353 227 118.13 1.320 233 111.69 1.248 187 105.19 1.175 83 89.13 0.996 631 82.69 0.924 1000 76.38 0.853 253 75.50 0.844 252
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