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5586-15-2

DI-2-NAPHTHYLDISULPHIDE

Product Name DI-2-NAPHTHYLDISULPHIDE

CAS5586-15-2

MFC20H14S2

MW318.46

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  • 5586-15-2_ms_1
    Mass

    MS-IW-9215          
    di(2-naphthyl) disulfide
    C20H14S2            (Mass of molecular ion:    318)
    

       Source Temperature: 180 °C
       Sample Temperature: 140 °C
       Direct, 75 eV
    

          39.0       1.9
          45.0       1.0
          50.0       1.1
          51.0       1.9
          62.0       1.1
          63.0       3.6
          65.0       2.2
          67.0       1.2
          69.0       1.8
          74.0       1.2
          75.0       2.0
          76.0       1.1
          77.0       1.7
          79.0       3.4
          80.0       2.0
          88.0       1.2
          89.0       4.7
         101.0       1.0
         113.0       2.2
         114.0       5.8
         115.0     100.0
         116.0      13.2
         126.0       2.5
         127.0       3.3
         128.0       6.8
         134.0       1.0
         158.0       6.8
         159.0      83.0
         160.0      33.5
         161.0       7.0
         162.0       1.6
         190.0       2.8
         252.0       1.9
         253.0       5.3
         254.0      33.3
         255.0       7.3
         282.0       1.0
         284.0       3.4
         285.0       5.8
         286.0       2.2
         316.0       1.8
         318.0      53.8
         319.0      12.6
         320.0       6.0
         321.0       1.1
    

400 MHz at 50C

  • 5586-15-2_1hnmr_0

    1H NMR 399.65 MHz
    C20 H14 S2 0.035 g : 0.5 ml CDCl3 at 50C
    di(2-naphthyl) disulfide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.960 B 7.735 C 7.74 D 7.686 E 7.602 F 7.42 G 7.40

         Hz     ppm     Int.
    

       3181.64   7.962    495
       3180.91   7.960    484
       3180.18   7.958    528
       3099.98   7.757    256
       3099.12   7.755    250
       3096.44   7.748    525
       3093.51   7.741    246
       3090.45   7.733    292
       3087.40   7.726    616
       3083.50   7.716     48
       3082.52   7.714     41
       3076.78   7.699    248
       3076.42   7.698    249
       3073.73   7.692    215
       3071.90   7.687    111
       3071.17   7.685    131
       3067.26   7.675    283
       3066.89   7.674    280
       3064.33   7.668     51
       3043.09   7.615    529
       3041.14   7.610    518
       3034.42   7.593    389
       3032.47   7.588    395
       2972.05   7.437    146
       2970.34   7.433     30
       2967.04   7.425    466
       2964.84   7.419    771
       2961.18   7.410   1000
       2957.40   7.400    732
       2955.44   7.396    453
       2952.39   7.388     31
       2952.03   7.387     30
       2950.44   7.383    151