2-Nitrobenzaldehyde

Mass

MS-NW-7213          
o-nitrobenzaldehyde
C7H5NO3             (Mass of molecular ion:    151)

   Source Temperature: 220 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       4.8
      28.0       3.8
      29.0       4.4
      30.0       7.0
      37.0       4.3
      38.0       5.1
      39.0      24.9
      40.0       1.1
      49.0       2.5
      50.0      34.5
      51.0      54.3
      52.0       6.5
      53.0       4.1
      61.0       2.1
      62.0       2.7
      63.0       4.9
      64.0       3.9
      65.0      77.1
      66.0       4.6
      73.0       2.2
      74.0      10.9
      75.0      10.2
      76.0      45.2
      77.0      24.8
      78.0       2.8
      79.0       1.3
      91.0       1.0
      92.0       1.9
      93.0      56.3
      94.0       4.0
     104.0      27.2
     105.0       3.4
     121.0     100.0
     122.0       8.3
     134.0       2.1

Parameter ppm Hz D(A) 8.15 D(B) 7.75 D(C) 7.78 D(D) 7.88 D(E) 10.03 J(A,B) 8.18 J(A,C) 1.15 J(A,D) 0.45 J(A,E) 0.30 J(B,C) 7.44 J(B,D) 1.49 J(B,E) 0.0 J(C,D) 7.69 J(C,E) 0.30 J(D,E) 0.0 SMITH,W.B. ET AL. J.AM.CHEM.SOC. 94, 1959 (1972) THE VALUES OF J(A,E) AND J(C,E) ARE OBTAINED FROM : CONTRERAS,R.H. ET AL. ORG.MAGN.RESON. 12, 542 (1979)

     Hz     ppm     Int.

   3009.02  10.030   1000
   2454.36   8.181     12
   2449.77   8.166    215
   2448.32   8.161    149
   2447.01   8.157    127
   2442.67   8.142    240
   2440.50   8.135    249
   2435.35   8.118     19
   2369.03   7.897    168
   2366.79   7.889    196
   2362.95   7.876    176
   2361.60   7.872    209
   2360.04   7.867    299
   2355.39   7.851     26
   2343.09   7.810     70
   2341.35   7.804    109
   2335.72   7.786    298
   2333.98   7.780    286
   2331.94   7.773    315
   2329.18   7.764    502
   2326.68   7.756    197
   2324.38   7.748    280
   2322.42   7.741    231
   2316.99   7.723     84
   2315.06   7.717     60