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MS-NW-9292 2,6-difluoroaniline C6H5F2N (Mass of molecular ion: 129)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
28.0 2.7 31.0 2.9 38.0 1.3 39.0 1.1 50.0 1.5 51.0 4.0 52.0 3.9 54.5 1.0 56.0 1.9 57.0 4.4 61.0 1.0 62.0 4.3 63.0 4.6 64.0 1.0 64.5 5.7 65.0 1.2 70.0 1.2 75.0 3.7 76.0 1.6 81.0 5.1 82.0 21.1 83.0 3.5 89.0 8.1 90.0 1.3 99.0 1.1 101.0 15.9 102.0 9.8 103.0 1.1 108.0 3.5 109.0 26.3 110.0 2.2 128.0 4.9 129.0 100.0 130.0 7.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H5 F2 N 0.05 ml : 0.5 ml CDCl3 2,6-difluoroaniline Assign. Shift(ppm)
A 6.778 B 6.576 C 3.73
Hz ppm Int.
2728.52 6.828 60 2726.56 6.823 67 2721.56 6.810 49 2720.46 6.808 91 2717.29 6.800 441 2716.92 6.799 436 2715.45 6.795 365 2714.84 6.794 339 2710.69 6.783 351 2710.08 6.782 412 2708.62 6.778 1000 2706.79 6.773 706 2702.03 6.761 642 2700.07 6.757 661 2697.02 6.749 73 2690.92 6.734 74 2688.35 6.727 53 2641.97 6.611 253 2635.86 6.596 486 2634.03 6.591 258 2633.18 6.589 229 2631.35 6.585 50 2629.64 6.580 274 2627.81 6.576 466 2627.20 6.574 450 2625.24 6.569 197 2623.41 6.565 41 2621.70 6.560 243 2620.85 6.558 227 2619.14 6.554 331 2612.92 6.539 169 1490.48 3.730 198
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