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MS-NW-2439 1,3-diphenylisobenzofuran C20H14O (Mass of molecular ion: 270)
Source Temperature: 190 °C Sample Temperature: 120 °C Direct, 75 eV
17.0 2.2 18.0 9.7 27.0 1.3 28.0 1.9 39.0 4.1 50.0 2.7 51.0 9.6 62.0 1.8 63.0 4.5 65.0 1.0 74.0 2.3 75.0 2.2 76.0 1.6 77.0 14.9 78.0 1.1 86.0 1.8 87.0 2.7 88.0 1.2 89.0 2.1 94.5 1.1 98.0 1.1 99.0 1.0 105.0 3.6 106.5 1.6 107.0 1.0 107.5 1.4 113.0 3.0 115.0 3.0 119.0 1.4 119.5 4.2 120.0 2.0 126.0 2.0 134.0 1.3 135.0 10.0 135.5 2.3 137.0 1.2 138.0 1.0 139.0 4.9 162.0 1.0 163.0 8.1 164.0 8.4 165.0 30.8 166.0 4.3 189.0 1.6 193.0 12.0 194.0 1.9 202.0 2.0 209.0 1.6 213.0 1.8 215.0 4.6 226.0 3.3 227.0 1.0 237.0 1.4 238.0 1.3 239.0 17.6 240.0 7.9 241.0 31.5 242.0 7.1 252.0 2.4 253.0 1.5 254.0 1.1 268.0 2.1 269.0 7.5 270.0 100.0 271.0 20.7 272.0 2.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C20 H14 O 16.8 mg : 0.5 ml CDCl3 1,3-diphenylisobenzofuran Assign. Shift(ppm)
A 7.943 B 7.836 C 7.479 D 7.290 E 7.016
Hz ppm Int.
3182.74 7.964 42 3179.93 7.957 784 3178.71 7.954 903 3176.76 7.949 272 3175.17 7.945 89 3173.22 7.940 329 3172.24 7.938 550 3171.51 7.936 968 3170.29 7.933 829 3168.58 7.929 174 3166.14 7.923 55 3165.04 7.920 39 3141.48 7.861 51 3139.40 7.856 82 3136.96 7.850 586 3134.16 7.843 378 3130.25 7.833 363 3127.08 7.825 612 3124.63 7.819 104 3122.56 7.814 67 3000.85 7.509 36 3000.24 7.508 35 2999.88 7.507 34 2998.17 7.502 153 2996.70 7.499 593 2994.87 7.494 241 2993.53 7.491 84 2993.04 7.490 75 2989.26 7.480 1000 2988.65 7.479 848 2985.72 7.471 88 2985.23 7.470 83 2984.74 7.469 81 2982.67 7.464 297 2981.08 7.460 679 2979.37 7.455 142 2977.66 7.451 46 2976.93 7.449 40 2921.51 7.311 214 2920.29 7.308 377 2919.07 7.305 208 2917.11 7.300 40 2916.63 7.298 43 2914.43 7.293 244 2912.96 7.289 577 2911.38 7.285 193 2909.06 7.280 48 2908.08 7.277 47 2906.62 7.273 168 2905.40 7.270 268 2904.30 7.268 146 2813.11 7.039 58 2811.16 7.035 91 2808.72 7.028 633 2805.91 7.021 368 2803.96 7.017 53 2801.88 7.011 377 2798.83 7.004 602 2797.61 7.001 62 2796.39 6.998 92 2795.65 6.996 48 2794.43 6.993 61
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