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5446-92-4

2-Methoxy-5-nitropyridine

Product Name 2-Methoxy-5-nitropyridine

CAS5446-92-4

MFC6H6N2O3

MW154.12

More

  • 5446-92-4_ms_1
    Mass

    MS-NW-6700          
    2-methoxy-5-nitropyridine
    C6H6N2O3            (Mass of molecular ion:    154)
    

       Source Temperature: 260 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          15.0       5.9
          18.0       2.1
          26.0       5.7
          27.0       7.8
          28.0       9.1
          29.0       3.1
          30.0       9.2
          37.0       8.6
          38.0      29.3
          39.0      20.8
          40.0       2.0
          41.0       1.8
          42.0       7.6
          46.0       2.9
          49.0       2.2
          50.0      15.4
          51.0      20.7
          52.0       9.5
          53.0      17.7
          54.0       4.2
          55.0       4.5
          63.0       2.7
          64.0      10.3
          65.0      13.7
          66.0      26.1
          67.0       2.9
          68.0       2.5
          69.0       3.0
          75.0       3.5
          76.0       5.6
          77.0       4.8
          78.0      41.8
          79.0      11.0
          80.0       5.7
          81.0      18.1
          82.0       2.2
          90.0       2.5
          93.0      38.3
          94.0       3.0
          96.0       3.3
         107.0      11.4
         108.0      35.6
         109.0       4.7
         123.0       1.8
         124.0      52.3
         125.0      27.3
         126.0       2.0
         138.0       2.9
         153.0      87.1
         154.0     100.0
         155.0       8.4
    

90 MHz in CDCl3

  • 5446-92-4_1hnmr_0

    1H NMR 89.56 MHz
    C6 H6 N2 O3 0.042 g : 0.5 ml CDCl3
    2-methoxy-5-nitropyridine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.077 B 8.341 C 6.829 D 4.055 J(A,B)=2.8HZ, J(A,C)=0.6HZ, J(B,C)=9.1HZ

         Hz     ppm     Int.
    

        814.38   9.094     45
        811.81   9.065     50
        753.38   8.413     73
        750.56   8.381     68
        744.25   8.311     82
        741.44   8.279     79
        616.25   6.881     73
        615.69   6.875     75
        607.13   6.780     63
        606.56   6.773     67
        363.19   4.056   1000
    

in CDCl3

  • 5446-92-4_13cnmr_0

KBr disk

  • 5446-92-4_ir1_2

nujol mull

  • 5446-92-4_ir2_1

  • 5446-92-4_raman