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MassMS-KW-0243 butyl nitrite C4H9NO2 (Mass of molecular ion: 103)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 3.0 18.0 2.8 19.0 1.0 26.0 4.0 27.0 55.1 28.0 13.8 29.0 35.0 30.0 63.7 31.0 26.3 33.0 2.0 37.0 1.1 38.0 2.2 39.0 18.2 40.0 3.3 41.0 95.7 42.0 14.4 43.0 100.0 44.0 13.5 45.0 2.8 53.0 1.5 54.0 1.2 55.0 8.6 56.0 33.1 57.0 34.2 58.0 1.6 60.0 57.4 61.0 1.1 71.0 8.8 72.0 5.9 73.0 2.5 89.0 3.3
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C4 H9 N O2 0.04 ml : 0.5 ml CDCl3 butyl nitrite 
Assign. Shift(ppm)
A 4.697 B 1.68 C 1.40 D 0.956
Hz ppm Int.427.63 4.775 318 421.19 4.703 751 414.69 4.631 434 169.69 1.895 50 168.06 1.877 51 167.69 1.873 45 163.38 1.825 98 162.75 1.818 93 161.63 1.805 139 161.25 1.801 141 159.38 1.780 92 158.75 1.773 75 157.81 1.763 97 156.75 1.751 97 154.75 1.728 291 153.75 1.717 202 152.94 1.708 186 152.13 1.699 155 151.00 1.687 97 150.50 1.681 61 148.19 1.655 279 147.31 1.645 232 146.38 1.635 181 145.56 1.626 116 143.56 1.603 178 142.56 1.592 141 142.00 1.586 173 141.50 1.580 153 140.69 1.571 126 140.06 1.564 104 138.13 1.543 166 137.38 1.534 171 136.94 1.530 203 136.19 1.521 227 135.69 1.516 136 134.31 1.500 86 133.94 1.496 82 133.38 1.490 99 132.00 1.474 182 131.00 1.463 233 130.00 1.452 192 128.69 1.437 289 127.06 1.419 96 126.50 1.413 101 126.06 1.408 90 125.06 1.397 148 124.56 1.391 163 124.06 1.386 170 121.94 1.362 310 121.06 1.352 145 119.44 1.334 91 118.25 1.321 93 117.19 1.309 40 116.56 1.302 42 115.38 1.289 236 114.19 1.276 139 112.75 1.259 45 108.94 1.217 118 102.13 1.141 77 101.56 1.134 57 94.31 1.054 49 93.13 1.040 393 91.94 1.027 641 91.25 1.019 630 90.44 1.010 308 88.63 0.990 88 88.00 0.983 81 87.56 0.978 72 85.44 0.954 1000 85.06 0.950 844 84.00 0.938 563 82.31 0.920 205 80.31 0.897 125 79.81 0.892 167 79.44 0.888 173 79.06 0.883 203 78.00 0.871 302 76.13 0.851 190
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1H NMR 399.65 MHz C4H9NO2 0.05 ml : 0.5 ml CDCl3 butyl nitrite Assign. Shift(ppm)
A 4.706 B 1.724 C 1.414 D 0.958
Hz ppm Int.1881.11 4.706 108 703.01 1.759 78 696.42 1.742 184 693.36 1.735 69 689.09 1.724 220 681.16 1.704 193 674.57 1.688 90 583.87 1.461 63 576.54 1.443 179 570.68 1.428 105 568.97 1.424 248 563.36 1.410 105 561.28 1.404 263 555.91 1.391 53 553.96 1.386 177 546.51 1.368 60 463.63 1.160 14 456.06 1.141 24 448.49 1.122 13 389.78 0.975 581 382.33 0.957 1000 375.01 0.939 495 318.97 0.798 12
in CDCl3
liquid film
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