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6-Methyl-1,3,5-triazine-2,4-diamine

Product Name 6-Methyl-1,3,5-triazine-2,4-diamine

CAS542-02-9

MFC4H7N5

MW125.13

¹³CNMR

Mass

MS-NW-0250          
6-methyl-1,3,5-triazine-2,4-diamine
C4H7N5              (Mass of molecular ion:    125)

   Source Temperature: 200 °C
   Sample Temperature:   0 °C
   Direct, 75 eV

      15.0       3.0
      18.0       1.8
      27.0       1.4
      28.0       6.8
      40.0       2.1
      41.0       4.0
      42.0      24.5
      43.0      57.5
      44.0       1.0
      53.0       1.4
      55.0       2.5
      58.0       1.1
      67.0       1.2
      68.0       6.0
      82.0       1.7
      83.0       6.9
      84.0       7.0
      85.0       2.7
      98.0       8.3
     110.0       2.0
     125.0     100.0
     126.0       9.6

400 MHz in DMSO-d6

90 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₄ H₇ N₅	saturated in DMSO-d₆
6-methyl-1,3,5-triazine-2,4-diamine

    Assign.     Shift(ppm)

      A             6.6
      B             2.064

     Hz     ppm     Int.

   2651.86   6.636     38
    825.20   2.065   1000

¹H NMR	89.56 MHz
C₄ H₇ N₅	0.044 g : 0.5 ml DMSO-d₆
6-methyl-1,3,5-triazine-2,4-diamine

    Assign.     Shift(ppm)

      A             6.61
      B             2.066

     Hz     ppm     Int.

    591.58   6.606    236
    185.08   2.067   1000

in DMSO-d6

KBr disc

nujol mull

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