5,6-DICHLORO-3-PYRIDINEMETHANOL

Mass

MS-IW-8669          
(5,6-dichloro-3-pyridyl)methanol
C6H5Cl2NO           (Mass of molecular ion:    177)

   Source Temperature: 210 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       2.3
      26.0       1.5
      27.0       3.1
      28.0       7.4
      29.0       7.8
      31.0      12.9
      32.0       1.2
      36.0       2.9
      37.0       3.1
      38.0       3.8
      39.0       4.1
      41.0       1.1
      43.0       1.0
      47.0       1.5
      48.0       1.9
      49.0       5.2
      50.0      12.1
      51.0      17.2
      52.0       4.5
      53.0       2.5
      55.0       3.4
      56.5       1.0
      57.0       1.3
      60.0       2.5
      61.0       4.1
      62.0       5.7
      63.0       4.5
      64.0       1.8
      69.0       1.2
      70.5       2.5
      72.0       2.4
      73.0       5.4
      74.0       2.1
      75.0       6.9
      76.0      22.1
      77.0       3.0
      78.0      23.3
      79.0       3.2
      83.0       1.2
      84.0       5.8
      85.0      11.7
      86.0       5.1
      87.0      10.2
      88.0       3.7
      89.0       3.5
      90.0       1.2
      91.0       1.8
      92.0       1.1
      96.0       1.1
      97.0       4.6
      98.0       1.4
      99.0       2.7
     105.0       1.4
     106.0      15.1
     107.0       3.1
     109.0       2.1
     110.0       7.1
     111.0       2.5
     112.0      77.7
     113.0      12.8
     114.0      35.3
     115.0      11.4
     116.0       4.2
     117.0       2.4
     119.0       1.5
     121.0       2.3
     123.0       1.2
     124.0      12.9
     125.0       4.3
     126.0       4.8
     127.0       1.4
     133.0       3.2
     134.0       1.0
     135.0       2.6
     140.0       6.4
     141.0       3.4
     142.0      37.6
     143.0       3.7
     144.0      11.7
     146.0       6.0
     147.0       5.0
     148.0     100.0
     149.0       9.4
     150.0      62.6
     151.0       4.5
     152.0      10.1
     159.0       6.4
     160.0       9.5
     161.0       5.4
     162.0       6.2
     163.0       1.4
     164.0       1.2
     174.0       4.9
     175.0       2.5
     176.0      56.7
     177.0      87.2
     178.0      42.0
     179.0      55.7
     180.0      10.2
     181.0       9.2

Assign. Shift(ppm) A 8.218 B 7.835 C 4.728 D 3.38

     Hz     ppm     Int.

   3285.40   8.221    414
   3284.79   8.220    294
   3284.06   8.218    296
   3283.33   8.216    419
   3133.06   7.840    280
   3132.32   7.838    486
   3131.59   7.836    308
   3130.98   7.835    305
   3130.25   7.833    462
   3129.52   7.831    254
   1889.65   4.729   1000
   1351.56   3.382     44