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ethyl N-(4-chlorophenyl)-2-oxoglycinate

Product Name ethyl N-(4-chlorophenyl)-2-oxoglycinate

CAS5397-14-8

MFC10H10ClNO3

MW227.64


  • Mass

    MS-NW-8061          
    ethyl 4'-chlorooxanilate
    C10H10ClNO3         (Mass of molecular ion:    227)
    

       Source Temperature: 180 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          18.0       2.4
          26.0       1.0
          27.0       9.2
          28.0       4.4
          29.0      72.7
          30.0       2.1
          37.0       1.1
          38.0       2.7
          39.0       3.9
          45.0       6.1
          45.5       2.3
          50.0       4.9
          51.0       2.7
          52.0       1.6
          61.0       1.4
          62.0       3.4
          63.0      10.9
          64.0       5.6
          65.0       3.7
          73.0       7.3
          74.0       3.6
          75.0      16.6
          76.0       4.1
          77.0       1.8
          85.0       1.4
          89.0       1.4
          90.0       9.0
          91.0       6.4
          92.0       3.3
          93.0       1.0
          99.0      20.6
         100.0       4.6
         101.0       6.9
         102.0       1.6
         105.0       1.0
         111.0      18.2
         112.0       2.0
         113.0       6.4
         119.0       1.5
         120.0       1.9
         125.0       6.2
         126.0      70.8
         127.0      36.8
         128.0      25.6
         129.0      11.3
         130.0       1.0
         139.0       1.8
         140.0      14.2
         141.0       1.7
         142.0       4.6
         153.0      70.9
         154.0      88.5
         155.0      37.9
         156.0      29.5
         157.0       5.1
         227.0     100.0
         228.0      12.3
         229.0      33.1
         230.0       4.0
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H10 Cl N O3 0.030 g : 0.5 ml CDCl3
    ethyl 4'-chlorooxanilate
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.96 B 7.615 C 7.339 D 4.410 E 1.417

         Hz     ppm     Int.
    

       3579.47   8.957     73
       3051.27   7.635     54
       3048.34   7.628    436
       3046.26   7.623    161
       3041.50   7.611    170
       3039.43   7.606    521
       3036.38   7.598     77
       2940.19   7.357     68
       2937.26   7.350    505
       2935.18   7.345    172
       2930.42   7.333    157
       2928.34   7.328    432
       2925.42   7.320     61
       1773.68   4.439    156
       1766.48   4.421    480
       1759.28   4.403    488
       1752.20   4.385    168
        573.73   1.436    491
        566.53   1.418   1000
        559.33   1.400    496
    

in CDCl3



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