NALPHA,NOMEGA-DICARBOBENZOXY-L-ARGININE

Mass

MS-NW-2409          
N(alpha),N(omega)-bis(benzyloxycarbonyl)-L-arginine
C22H26N4O6          (Mass of molecular ion:    442)

   Source Temperature: 260 °C
   Sample Temperature: 240 °C
   Direct, 75 eV

      16.0       2.2
      17.0       3.4
      18.0      17.2
      26.0       2.6
      27.0       8.1
      28.0      21.4
      29.0       4.7
      30.0       1.9
      31.0       3.2
      37.0       2.1
      38.0       3.5
      39.0      13.4
      40.0       1.7
      41.0       3.3
      42.0       2.8
      43.0       4.4
      44.0      48.8
      49.0       1.2
      50.0      10.5
      51.0      22.3
      52.0       7.1
      53.0       5.4
      53.5       1.5
      54.0       1.8
      55.0       1.6
      56.0       1.5
      61.0       1.8
      62.0       2.5
      63.0       6.1
      64.0       1.7
      65.0       9.5
      66.0       1.1
      68.0       1.0
      69.0       3.4
      70.0       1.9
      74.0       3.0
      75.0       1.8
      76.0       1.7
      77.0      52.5
      78.0      13.5
      79.0     100.0
      80.0      10.8
      85.0       1.0
      89.0       6.9
      90.0       9.3
      91.0      29.0
      92.0       4.7
      97.0       1.4
      99.0       1.5
     105.0       7.7
     106.0       5.2
     107.0      64.8
     108.0      90.8
     109.0       7.2
     110.0       1.0
     113.0       1.0
     141.0       1.6

Assign. Shift(ppm) A 7.35 B 5.03 C 3.94 D 3.11 E *1 1.72 F *1 1.53

     Hz     ppm     Int.

   2939.00   7.354    741
   2937.16   7.350    376
   2935.49   7.346    353
   2931.82   7.336   1000
   2008.97   5.027    437
   1566.47   3.920     44
   1244.81   3.115     67
    687.41   1.721     31
    611.57   1.531     47