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2-BROMO-N,N-DIETHYLETHYLAMINE HYDROBROMIDE

Product Name 2-BROMO-N,N-DIETHYLETHYLAMINE HYDROBROMIDE

CAS5392-81-4

MFC6H14BrN

MW180.09

Mass

MS-NW-6609          
2-bromotriethylamine hydrobromide
C6H14BrN HBr        (Mass of molecular ion:    179)

   Source Temperature: 150 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      15.0       3.5
      17.0       1.0
      18.0       4.3
      26.0       2.4
      27.0      20.5
      28.0      14.8
      29.0      17.4
      30.0      16.1
      39.0       1.0
      40.0       1.0
      41.0       4.3
      42.0      18.3
      43.0       3.1
      44.0      41.2
      45.0       1.0
      54.0       2.3
      55.0       1.9
      56.0      12.6
      57.0       4.7
      58.0      14.1
      70.0       4.5
      71.0       3.6
      72.0      19.0
      79.0       9.8
      80.0      29.7
      81.0       9.9
      82.0      28.3
      84.0       2.4
      85.0       1.2
      86.0     100.0
      87.0       6.2
      98.0       1.0
      99.0       1.2
     100.0      65.0
     101.0       5.0
     107.0       7.9
     108.0       1.7
     109.0       6.7
     110.0       1.6
     122.0       1.0
     136.0       5.0
     138.0       5.0
     164.0      11.8
     166.0      11.0
     178.0       1.1
     179.0      10.9
     180.0       1.9
     181.0      10.5

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₁₄ Br N	0.039 g : 0.5 ml DMSO-d₆
2-bromotriethylamine hydrobromide

    Assign.     Shift(ppm)

      A             9.77
      B             3.853
      C             3.54
      D             3.22
      E             1.231

     Hz     ppm     Int.

   1547.70   3.873    131
   1543.88   3.864     32
   1540.68   3.856    226
   1539.46   3.853    138
   1536.10   3.844     33
   1532.75   3.836    164
   1423.19   3.562     72
   1418.15   3.549     85
   1415.41   3.542    108
   1410.37   3.530    105
   1408.39   3.525     68
   1403.20   3.512     55
   1303.41   3.262     31
   1302.19   3.259     37
   1300.96   3.256     35
   1294.86   3.240    103
   1290.28   3.229    103
   1287.38   3.222    129
   1286.77   3.220    126
   1282.96   3.211    119
   1281.74   3.208    119
   1279.30   3.202    110
   1274.41   3.189    104
   1268.31   3.174     42
   1267.24   3.171     48
    499.27   1.250    464
    492.10   1.232   1000
    484.77   1.213    443

KBr disc

nujol mull

4880 A,200 M,powder

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