2'-DIMETHYLAMINO-5'-NITROACETANILIDE

Mass

MS-IW-1287          
2'-dimethylamino-5'-nitroacetanilide
C10H13N3O3          (Mass of molecular ion:    223)

   Source Temperature: 180 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      15.0       3.8
      17.0       1.1
      18.0       5.3
      27.0       2.0
      28.0       4.6
      30.0       6.2
      39.0       3.0
      41.0       1.8
      42.0       7.3
      43.0      18.3
      44.0       8.4
      50.0       1.1
      51.0       2.4
      52.0       2.4
      63.0       2.7
      64.0       1.9
      65.0       4.8
      66.0       1.9
      67.0       1.1
      76.0       1.3
      77.0       2.3
      78.0       2.8
      79.0       1.5
      80.0       1.1
      90.0       1.4
      91.0       3.1
      92.0       9.5
      93.0       3.2
      94.0       2.7
     104.0       1.7
     105.0       2.7
     106.0       3.8
     107.0       2.3
     108.0       2.6
     117.0       1.8
     118.0       5.2
     119.0       9.2
     120.0       5.8
     121.0       1.1
     122.0       1.5
     131.0       2.4
     132.0       8.0
     133.0       9.6
     134.0      28.2
     135.0       6.9
     136.0       2.5
     138.0       1.2
     145.0       1.0
     146.0       1.6
     147.0       5.5
     148.0       2.0
     149.0       2.1
     150.0       1.1
     151.0       2.7
     152.0       2.7
     161.0       1.8
     162.0       7.4
     163.0       6.9
     164.0      14.2
     165.0      15.9
     166.0      35.3
     167.0       3.0
     175.0       1.8
     176.0       2.2
     177.0       6.4
     178.0       4.5
     179.0       1.3
     180.0      87.5
     181.0      22.0
     182.0       2.3
     190.0       1.7
     191.0       3.0
     192.0       1.0
     193.0       5.1
     194.0       1.2
     204.0       1.0
     205.0       1.8
     206.0      10.7
     207.0       3.3
     208.0       7.8
     223.0     100.0
     224.0      13.7
     225.0       1.5

Assign. Shift(ppm) A 9.09 B 8.1 C 7.908 D 7.164 E 2.754 F 2.269

     Hz     ppm     Int.

    815.00   9.101     39
    812.31   9.071     40
    714.44   7.978     47
    711.75   7.948     45
    705.63   7.879     57
    702.94   7.849     55
    645.50   7.208     84
    636.69   7.110     65
    246.75   2.756   1000
    203.25   2.270    554