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5350-57-2

Benzophenone hydrazone

Product Name Benzophenone hydrazone

CAS5350-57-2

MFC13H12N2

MW196.25

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  • 5350-57-2_ms_1
    Mass

    MS-NW-9495          
    benzophenone hydrazone
    C13H12N2            (Mass of molecular ion:    196)
    

       Source Temperature: 150 °C
       Sample Temperature:  80 °C
       Direct, 75 eV
    

          18.0       2.2
          28.0       1.1
          39.0       2.0
          50.0       2.4
          51.0      11.3
          52.0       1.1
          63.0       2.5
          65.0       2.6
          66.0       2.4
          69.5       1.1
          74.0       1.2
          75.0       1.5
          76.0       4.2
          77.0      38.6
          78.0       3.3
          82.0       1.9
          82.5       2.2
          83.0       1.1
          83.5       1.3
          89.0       1.5
          91.0       3.0
          92.0       5.2
          93.0       9.1
          98.0       1.6
         103.0       2.0
         104.0       1.9
         115.0       1.8
         118.0       6.5
         119.0      11.2
         139.0       2.1
         151.0       2.3
         152.0       4.8
         153.0       1.7
         163.0       2.1
         164.0       2.5
         165.0      36.6
         166.0       7.4
         167.0       2.5
         168.0       1.5
         178.0       5.4
         179.0      11.8
         180.0      20.7
         181.0       3.6
         195.0      37.3
         196.0     100.0
         197.0      15.3
         198.0       1.0
    

400 MHz in CDCl3

  • 5350-57-2_1hnmr_0

    1H NMR 399.65 MHz
    C13 H12 N2 0.041 g : 0.5 ml CDCl3
    benzophenone hydrazone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.510 B 7.47 C 7.44 D 7.28 E 7.27 F 7.25 G 5.42

         Hz     ppm     Int.
    

       3011.35   7.535    201
       3010.13   7.532    356
       3008.54   7.528    144
       3004.88   7.519    241
       3003.17   7.515    733
       3001.71   7.511    454
       2999.27   7.505     66
       2996.95   7.499    297
       2995.73   7.496    600
       2994.87   7.494    439
       2993.65   7.491    153
       2992.31   7.488     80
       2989.01   7.480    564
       2987.79   7.477    238
       2986.69   7.474    369
       2986.08   7.472    344
       2984.86   7.469    271
       2983.76   7.466    288
       2982.91   7.464    346
       2980.96   7.459    923
       2979.25   7.455    859
       2977.29   7.450    106
       2975.59   7.446    178
       2973.14   7.440    398
       2970.83   7.434    113
       2967.29   7.425     93
       2965.82   7.422    150
       2964.48   7.418     78
       2921.14   7.310     35
       2918.21   7.302    150
       2914.92   7.294    797
       2913.45   7.291    964
       2911.38   7.285    304
       2909.67   7.281    604
       2909.06   7.280    666
       2908.45   7.278    625
       2907.35   7.275    680
       2906.62   7.273    887
       2905.76   7.271    740
       2905.40   7.270    731
       2903.20   7.265   1000
       2901.73   7.261    963
       2898.68   7.254    254
       2898.19   7.252    198
       2896.73   7.249    153
       2892.09   7.237     55
       2890.26   7.232    150
       2167.24   5.423    524
    

in CDCl3

KBr disc

nujol mull