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MassMS-NW-9495 benzophenone hydrazone C13H12N2 (Mass of molecular ion: 196)
Source Temperature: 150 °C Sample Temperature: 80 °C Direct, 75 eV
18.0 2.2 28.0 1.1 39.0 2.0 50.0 2.4 51.0 11.3 52.0 1.1 63.0 2.5 65.0 2.6 66.0 2.4 69.5 1.1 74.0 1.2 75.0 1.5 76.0 4.2 77.0 38.6 78.0 3.3 82.0 1.9 82.5 2.2 83.0 1.1 83.5 1.3 89.0 1.5 91.0 3.0 92.0 5.2 93.0 9.1 98.0 1.6 103.0 2.0 104.0 1.9 115.0 1.8 118.0 6.5 119.0 11.2 139.0 2.1 151.0 2.3 152.0 4.8 153.0 1.7 163.0 2.1 164.0 2.5 165.0 36.6 166.0 7.4 167.0 2.5 168.0 1.5 178.0 5.4 179.0 11.8 180.0 20.7 181.0 3.6 195.0 37.3 196.0 100.0 197.0 15.3 198.0 1.0
400 MHz in CDCl3
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1H NMR 399.65 MHz C13 H12 N2 0.041 g : 0.5 ml CDCl3 benzophenone hydrazone 
Assign. Shift(ppm)
A 7.510 B 7.47 C 7.44 D 7.28 E 7.27 F 7.25 G 5.42
Hz ppm Int.3011.35 7.535 201 3010.13 7.532 356 3008.54 7.528 144 3004.88 7.519 241 3003.17 7.515 733 3001.71 7.511 454 2999.27 7.505 66 2996.95 7.499 297 2995.73 7.496 600 2994.87 7.494 439 2993.65 7.491 153 2992.31 7.488 80 2989.01 7.480 564 2987.79 7.477 238 2986.69 7.474 369 2986.08 7.472 344 2984.86 7.469 271 2983.76 7.466 288 2982.91 7.464 346 2980.96 7.459 923 2979.25 7.455 859 2977.29 7.450 106 2975.59 7.446 178 2973.14 7.440 398 2970.83 7.434 113 2967.29 7.425 93 2965.82 7.422 150 2964.48 7.418 78 2921.14 7.310 35 2918.21 7.302 150 2914.92 7.294 797 2913.45 7.291 964 2911.38 7.285 304 2909.67 7.281 604 2909.06 7.280 666 2908.45 7.278 625 2907.35 7.275 680 2906.62 7.273 887 2905.76 7.271 740 2905.40 7.270 731 2903.20 7.265 1000 2901.73 7.261 963 2898.68 7.254 254 2898.19 7.252 198 2896.73 7.249 153 2892.09 7.237 55 2890.26 7.232 150 2167.24 5.423 524
in CDCl3
KBr disc
nujol mull
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