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2-Hydroxy-4-methylpyrimidine hydrochloride

Product Name 2-Hydroxy-4-methylpyrimidine hydrochloride

CAS5348-51-6

MFC5H7ClN2O

MW146.57

¹³CNMR

Mass

MS-KW-0420          
4-methyl-2-pyrimidinol hydrochloride
C5H6N2O HCl         (Mass of molecular ion:    110)

   Source Temperature: 190 °C
   Sample Temperature: 130 °C
   Direct, 75 eV

      15.0       1.9
      17.0       1.0
      18.0       5.2
      26.0       3.6
      27.0       2.7
      28.0      12.5
      29.0       1.3
      35.0       4.5
      36.0      72.4
      37.0       2.8
      38.0      26.6
      39.0      12.5
      40.0      13.9
      41.0       9.4
      42.0      19.1
      43.0       1.9
      44.0       5.4
      51.0       1.7
      52.0       4.0
      53.0       1.7
      54.0       3.4
      55.0       4.4
      64.0       1.0
      65.0       1.1
      66.0       4.7
      67.0       4.8
      68.0      16.2
      69.0       2.5
      81.0       3.9
      82.0      29.4
      83.0       1.8
      95.0      34.1
      96.0       1.9
     109.0       6.2
     110.0     100.0
     111.0       6.8

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₅H₆N₂O HCl	0.038 g : 0.5 ml DMSO-d₆
4-methyl-2-pyrimidinol hydrochloride

    Assign.     Shift(ppm)

     A           8.615
     B           6.826
     C           2.579

     Hz     ppm     Int.

   3446.90   8.622    181
   3440.68   8.607    185
   2731.69   6.833    160
   2725.47   6.818    158
   1030.64   2.579   1000

in DMSO-d6

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