3-Methyl-2-nitroanisole

Mass

MS-IW-8126          
3-methyl-2-nitroanisole
C8H9NO3             (Mass of molecular ion:    167)

   Source Temperature: 200 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.9
      27.0       2.6
      28.0       2.7
      29.0       1.1
      30.0       2.6
      37.0       1.2
      38.0       3.0
      39.0      14.8
      40.0       2.2
      41.0       4.0
      42.0       1.9
      43.0       1.3
      50.0       7.8
      51.0      19.5
      52.0      14.4
      53.0       9.3
      54.0       1.0
      55.0       1.8
      59.0       4.9
      61.0       1.3
      62.0       3.7
      63.0      10.6
      64.0       4.5
      65.0      40.3
      66.0      10.3
      67.0       4.3
      68.0       1.0
      74.0       2.2
      75.0       2.1
      76.0       3.3
      77.0      28.8
      78.0      26.9
      79.0       8.4
      80.0       4.0
      81.0       4.5
      89.0       7.3
      90.0      10.7
      91.0      60.5
      92.0      14.0
      93.0       7.9
      94.0      16.1
      95.0      27.4
      96.0       2.2
     104.0       1.3
     105.0      19.5
     106.0      17.9
     107.0       6.0
     108.0       5.3
     109.0       4.3
     118.0       1.5
     119.0       1.4
     120.0       7.8
     121.0       2.0
     122.0       7.7
     123.0       1.4
     135.0       8.0
     136.0       2.8
     137.0       1.6
     150.0      97.5
     151.0       9.4
     152.0       1.1
     167.0     100.0
     168.0       9.6
     169.0       1.0

Assign. Shift(ppm) A 7.284 B 6.86 C 3.868 D 2.294

     Hz     ppm     Int.

    661.88   7.391     48
    654.50   7.308     60
    653.13   7.293     62
    645.88   7.212     90
    618.31   6.904    101
    616.94   6.889    101
    616.25   6.881     93
    609.56   6.807     89
    608.94   6.800     80
    608.31   6.793     57
    607.75   6.786     41
    346.50   3.869   1000
    344.50   3.847     47
    205.50   2.295    555