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MS-NW-7253 N-ethylacetanilide C10H13NO (Mass of molecular ion: 163)
Source Temperature: 210 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.1 27.0 2.1 28.0 1.1 29.0 1.5 39.0 3.0 42.0 2.7 43.0 19.9 44.0 1.3 50.0 1.7 51.0 7.0 52.0 1.3 63.0 1.6 64.0 1.6 65.0 3.5 66.0 1.3 70.0 5.2 77.0 16.7 78.0 2.9 79.0 2.7 91.0 2.1 92.0 1.9 93.0 4.6 104.0 4.1 105.0 3.1 106.0 100.0 107.0 8.2 118.0 1.8 120.0 7.4 121.0 15.1 122.0 1.4 135.0 6.1 148.0 1.3 163.0 22.5 164.0 3.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H13 N O 0.048 g : 0.5 ml CDCl3 N-ethylacetanilide Assign. Shift(ppm)
A 7.55 to 7.290 B 7.18 C 3.752 D 1.826 E 1.116
Hz ppm Int.
676.19 7.551 35 674.19 7.528 30 672.19 7.506 62 670.50 7.487 55 667.31 7.451 205 666.25 7.440 151 665.38 7.430 152 664.25 7.417 154 662.38 7.396 325 661.50 7.387 403 659.94 7.369 517 656.88 7.335 181 655.00 7.314 123 654.63 7.310 120 652.94 7.291 40 652.00 7.281 48 650.63 7.265 52 649.13 7.248 66 647.69 7.232 99 645.88 7.212 423 644.75 7.200 142 643.19 7.182 229 641.13 7.159 178 640.06 7.147 135 638.19 7.126 213 636.19 7.104 198 347.19 3.877 128 340.00 3.797 402 337.13 3.765 32 332.88 3.717 425 325.75 3.638 153 169.88 1.897 31 163.56 1.827 930 156.81 1.751 37 156.25 1.745 35 106.88 1.194 491 104.06 1.162 45 99.81 1.115 1000 96.38 1.077 50 95.88 1.071 49 95.44 1.066 50 92.56 1.034 432
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