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Octyltrichlorosilane

Product Name Octyltrichlorosilane

CAS5283-66-9

MFC8H17Cl3Si

MW247.66

Mass

MS-NW-3330          
trichlorooctylsilane
C8H17Cl3Si          (Mass of molecular ion:    246)

   Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      27.0       8.8
      28.0       2.1
      29.0      14.7
      39.0       6.8
      40.0       1.3
      41.0      24.9
      42.0      11.8
      43.0     100.0
      44.0       3.2
      53.0       1.5
      54.0       1.3
      55.0      13.4
      56.0      12.4
      57.0      48.7
      58.0       2.4
      63.0       2.0
      65.0       1.0
      69.0       4.1
      70.0       4.3
      71.0      25.9
      72.0       1.6
      84.0       2.1
      85.0      40.4
      86.0       2.9
      98.0       1.4
      99.0       1.7
     100.0       1.1
     101.0       1.1
     117.0       1.1
     125.0       1.5
     127.0       1.1
     133.0      14.9
     135.0      15.0
     137.0       5.0
     139.0       2.9
     141.0       2.2
     153.0       2.8
     155.0       1.8
     161.0       5.3
     163.0       5.0
     165.0       1.7
     167.0       2.2
     169.0       1.3
     174.0       1.7
     175.0      13.0
     176.0       3.0
     177.0      13.4
     178.0       1.8
     179.0       4.8
     189.0       4.6
     190.0       1.1
     191.0       4.1
     193.0       1.4
     203.0       3.7
     204.0       1.0
     205.0       3.4
     207.0       1.3
     217.0       2.2
     219.0       2.3
     246.0       1.2
     248.0       1.2

90 MHz in CDCl3

400 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₇ Cl₃ Si	0.04 ml : 0.5 ml CDCl₃
trichlorooctylsilane

    Assign.     Shift(ppm)

      A          1.76 to 1.08
      B             0.89

     Hz     ppm     Int.

    154.25   1.723     36
    153.94   1.719     39
    153.31   1.712     39
    152.56   1.704     39
    152.19   1.700     41
    151.88   1.696     43
    151.25   1.689     43
    150.56   1.682     47
    148.75   1.661     62
    148.44   1.658     62
    147.88   1.652     63
    147.56   1.648     61
    146.25   1.633     70
    145.88   1.629     70
    145.38   1.624     73
    144.50   1.614     77
    143.44   1.602     85
    141.25   1.578    113
    134.94   1.507    252
    129.63   1.448    496
    127.06   1.419    372
    126.75   1.416    368
    125.63   1.403    367
    115.88   1.294    997
    115.19   1.287   1000
    104.19   1.164     39
    103.00   1.151     37
    102.44   1.144     36
    102.06   1.140     36
     84.63   0.945    167
     79.31   0.886    549
     73.25   0.818    114

¹H NMR	399.65 MHz
C₈ H₁₇ Cl₃ Si	0.05 ml : 0.5 ml CDCl₃
trichlorooctylsilane

    Assign.     Shift(ppm)

      A             1.58
      B          1.48 to 1.360
      C          1.36 to 1.210
      D             0.89

     Hz     ppm     Int.

    648.68   1.624     51
    647.09   1.620     50
    643.31   1.610     61
    641.60   1.606    127
    639.04   1.599    104
    636.96   1.594     95
    634.89   1.589    136
    633.30   1.585    191
    632.45   1.583    180
    630.00   1.577    101
    628.66   1.574    110
    627.32   1.570    136
    625.37   1.565    199
    622.19   1.557    121
    620.48   1.553     61
    617.68   1.546    105
    616.46   1.543    100
    584.72   1.464     31
    576.54   1.443     78
    576.05   1.442     79
    574.71   1.439     82
    569.21   1.425    179
    564.94   1.414    606
    562.01   1.407    271
    559.69   1.401    333
    556.88   1.394    348
    555.79   1.391    380
    548.83   1.374    288
    548.22   1.372    292
    544.19   1.362     64
    543.58   1.361     64
    530.52   1.328    215
    523.68   1.311    381
    518.68   1.298    545
    517.21   1.295    569
    515.14   1.289    655
    512.94   1.284    728
    365.72   0.916     60
    361.33   0.905    342
    354.61   0.888   1000
    347.53   0.870    379

liquid film

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