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1-HYDROXYPHENAZINE

Product Name 1-HYDROXYPHENAZINE

CAS528-71-2

MFC12H8N2O

MW196.2

Mass

MS-NW-1954          
1-phenazinol
C12H8N2O            (Mass of molecular ion:    196)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Reservoir, 75 eV

      17.0       1.2
      18.0       6.5
      28.0       2.3
      37.0       1.1
      38.0       2.6
      39.0       8.3
      50.0       4.1
      51.0       4.1
      52.0       1.7
      62.0       1.6
      63.0       4.6
      64.0       2.9
      65.0       1.4
      70.5       3.4
      75.0       2.5
      76.0       3.7
      77.0      13.7
      78.0       2.5
      83.5       1.1
      84.0       5.7
      90.0       1.3
      98.0       2.6
     102.0       2.3
     113.0       1.0
     114.0       2.3
     115.0       1.3
     118.0       1.1
     129.0       1.1
     140.0       4.3
     141.0       1.6
     142.0       2.8
     167.0       6.0
     168.0      57.3
     169.0       7.4
     196.0     100.0
     197.0      14.0
     198.0       1.2

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₈ N₂ O	saturated in CDCl₃
1-phenazinol

    Assign.     Shift(ppm)

      A             8.33
      B     *1      8.217
      C     *1      8.121
      D     *2      7.80
      E     *2      7.76
      F             7.75
      G             7.73
      J             7.209

     Hz     ppm     Int.

   3328.13   8.328    208
   3289.67   8.232    189
   3288.94   8.230    207
   3287.48   8.226    257
   3281.49   8.211    180
   3280.40   8.209    220
   3279.54   8.207    216
   3278.81   8.205    215
   3250.49   8.134    182
   3249.76   8.132    194
   3248.78   8.130    192
   3247.68   8.127    165
   3241.82   8.112    270
   3240.36   8.108    206
   3239.62   8.107    197
   3132.81   7.839     31
   3126.46   7.823    115
   3124.76   7.819    145
   3123.29   7.816     62
   3121.58   7.811     45
   3119.75   7.807    277
   3118.16   7.803    261
   3116.21   7.798    126
   3115.11   7.795     57
   3111.57   7.786    385
   3109.25   7.780    400
   3104.61   7.769    163
   3102.91   7.765    322
   3101.20   7.760    258
   3096.19   7.748    786
   3094.24   7.743   1000
   3087.77   7.727    502
   3085.45   7.721     64
   3078.86   7.704    145
   2885.38   7.220    344
   2883.42   7.215    313
   2878.91   7.204    301
   2876.83   7.199    308

¹H NMR	89.56 MHz
C₁₂ H₈ N₂ O	0.036 g : 0.5 ml CDCl₃
1-phenazinol

    Assign.     Shift(ppm)

      A          8.29 to 8.14
      B          7.88 to 7.71
      C             7.222

     Hz     ppm     Int.

    744.38   8.312     88
    743.63   8.304    110
    742.25   8.288     38
    741.00   8.274    127
    739.69   8.260    141
    738.44   8.246    187
    737.69   8.237    160
    736.00   8.218    163
    735.56   8.214    133
    734.19   8.198    150
    733.44   8.190    241
    731.19   8.165    143
    729.31   8.144     33
    728.19   8.131    169
    727.44   8.123    135
    725.06   8.096     48
    723.81   8.082     30
    708.69   7.914     71
    706.94   7.894     56
    705.00   7.872    265
    704.25   7.864    289
    702.94   7.849     41
    702.00   7.839    176
    700.38   7.821    209
    698.69   7.802    173
    697.06   7.784   1000
    694.38   7.754    330
    693.44   7.743    477
    692.13   7.729    476
    690.19   7.707     69
    683.19   7.629     45
    650.75   7.267    246
    647.13   7.226    181
    645.81   7.211    181
    642.13   7.170    169

KBr disc

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