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MS-NW-7299 6-methoxyquinoline C10H9NO (Mass of molecular ion: 159)
Source Temperature: 200 °C Sample Temperature: 190 °C Reservoir, 75 eV
38.0 1.7 39.0 3.7 50.0 2.6 51.0 3.0 52.0 1.5 61.0 1.1 62.0 4.0 63.0 9.0 64.0 2.3 65.0 1.2 74.0 2.4 75.0 3.2 76.0 1.7 77.0 2.2 79.5 2.1 87.0 1.2 88.0 2.7 89.0 17.1 90.0 3.4 101.0 2.8 102.0 3.4 103.0 1.1 114.0 1.0 115.0 1.9 116.0 66.9 117.0 6.6 128.0 4.3 129.0 14.3 130.0 5.1 144.0 11.4 145.0 1.5 158.0 1.2 159.0 100.0 160.0 11.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H9 N O 0.05 ml : 0.5 ml CDCl3 6-methoxyquinoline Assign. Shift(ppm)
A 8.731 B 7.98 C 7.95 D 7.33 E 7.28 F 6.982 G 3.864
Hz ppm Int.
784.94 8.765 82 783.31 8.747 88 780.69 8.717 89 779.06 8.699 89 720.56 8.046 96 717.94 8.017 62 716.44 8.000 60 716.06 7.996 60 711.38 7.944 141 709.88 7.927 89 708.06 7.906 78 662.94 7.403 93 660.13 7.371 108 657.19 7.338 109 653.69 7.299 99 652.94 7.291 113 650.94 7.269 101 648.88 7.246 81 644.56 7.197 71 626.44 6.995 137 623.75 6.965 119 344.50 3.847 1000
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