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5221-42-1

4-ACETAMIDOPYRIDINE

Product Name 4-ACETAMIDOPYRIDINE

CAS5221-42-1

MFC7H8N2O

MW136.15

More

  • 5221-42-1_ms
    Mass

    MS-IW-3941          
    N-(4-pyridyl)acetamide
    C7H8N2O             (Mass of molecular ion:    136)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          15.0       2.8
          26.0       1.4
          28.0       6.5
          37.0       1.2
          38.0       3.2
          39.0       8.8
          40.0       5.7
          41.0       7.1
          42.0       4.4
          43.0      57.3
          44.0       1.8
          50.0       2.8
          51.0       7.3
          52.0       4.7
          53.0       1.2
          54.0       1.9
          64.0       1.0
          65.0       1.4
          66.0       4.4
          67.0      35.4
          68.0       3.5
          77.0       1.0
          78.0       3.9
          93.0       5.5
          94.0     100.0
          95.0       7.8
         107.0       1.3
         108.0       5.4
         136.0      54.8
         137.0       4.9
    

in DMSO-d6

parameter in DMSO-d6

  • 5221-42-1_1hnmr_2

  • 5221-42-1_1hnmr

    1H NMR 300 MHz
    C7 H8 N2 O 30 % in DMSO
    N-(4-pyridyl)acetamide
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 8.54 D(B) 7.69 J(A,A') 0.4 J(A,B) 5.4 J(A,B') 0.8 J(A',B) 0.8 J(A',B') 5.4 J(B,B') 1.5 D(C) 10.5 D(D) 2.25 BRUEGEL,W. Z.ELEKTROCHEM.(BER.BUNSENGES.PHYS.CHEM.) 66, 159 (1962)

         Hz     ppm     Int.
    

       3150.00  10.500    333
       2565.13   8.550    223
       2563.83   8.546    132
       2560.32   8.534    136
       2559.02   8.530    236
       2310.10   7.700    233
       2308.73   7.696    132
       2305.29   7.684    129
       2303.92   7.680    222
        675.03   2.250   1000
    

in DMSO-d6

  • 5221-42-1_13cnmr

KBr disc

  • 5221-42-1_ir1_2

nujol mull

  • 5221-42-1_ir2